O,O-dimethyl carbonothioate

Base Information

• Chemical Name: O,O-dimethyl carbonothioate
• CAS No.: 1115-13-5
• Molecular Formula: C3H6 O2 S
• Molecular Weight: 106.145
• Mol file: 1115-13-5.mol

Synonyms:Carbonicacid, thio-, O,O-dimethyl ester (6CI,8CI); O,O-Dimethyl thiocarbonate;O,O'-Dimethyl thiocarbonate

Chemical Property of O,O-dimethyl carbonothioate

Chemical Property:

• Vapor Pressure: 130mmHg at 25°C
• Boiling Point: 72.4°C at 760 mmHg
• Density: 1.108g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of O,O-dimethyl carbonothioate

There total 3 articles about O,O-dimethyl carbonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methyl chlorothioformate (2812-72-8) + sodium methylate (124-41-4) → Dimethyl monothionocarbonate (1115-13-5)

Guidance literature:

In diethyl ether; Heating;

DOI:10.1021/jo00172a056

Reference yield:

thiophosgene (463-71-8) + sodium methylate (124-41-4) → Dimethyl monothionocarbonate (1115-13-5)

Guidance literature:

Reference yield:

→ Dimethyl monothionocarbonate (1115-13-5)

Guidance literature:

N,N'-Thiocarbonyl-di-imidazol, sd. Me., 30 min;

upstream raw materials:

thiophosgene

sodium methylate

methyl chlorothioformate

Downstream raw materials:

N,N-diphenylurea

bis-methoxycarbonyl-disulfane

dimexano

(methoxycarbonyl)(methoxy(thiocarbonyl))disulfane