dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate

Base Information

• Chemical Name: dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate
• CAS No.: 64377-83-9
• Molecular Formula: C₂₅H₃₃N₃O₅
• Molecular Weight: 455.554

Synonyms:1,2-Hydrazinedicarboxylicacid, 1-methyl-2-[5-[(1-methylethyl)amino]-5-oxopentyl]-, bis(phenylmethyl)ester (9CI); NSC 264082

Chemical Property of dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.161g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate

There total 3 articles about dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 5-bromovalerate (14660-52-7) → Bis(phenylmethyl)-1-methyl-2<5-<(1-methylethyl)amino>-5-oxopentyl>-1,2-hydrazindicarboxylat (64377-83-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: (i) aq. NaOH, EtOH, (ii) SOCl₂, (iii) /BRN= 605259/, THF

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1002/jps.2600660629

Reference yield:

1-methyl-1,2-dicarbobenzoxy-hydrazine (6002-83-1) → Bis(phenylmethyl)-1-methyl-2<5-<(1-methylethyl)amino>-5-oxopentyl>-1,2-hydrazindicarboxylat (64377-83-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: (i) aq. NaOH, EtOH, (ii) SOCl₂, (iii) /BRN= 605259/, THF

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1002/jps.2600660629

Reference yield:

Bis(phenylmethyl)-1-(5-ethoxy-5-oxopentyl)-2-methyl-1,2-hydrazindicarboxylat (64377-80-6) + isopropylamine (75-31-0) → Bis(phenylmethyl)-1-methyl-2<5-<(1-methylethyl)amino>-5-oxopentyl>-1,2-hydrazindicarboxylat (64377-83-9)

Guidance literature:

Multistep reaction; (i) aq. NaOH, EtOH, (ii) SOCl₂, (iii) /BRN= 605259/, THF;

DOI:10.1002/jps.2600660629

upstream raw materials:

Bis(phenylmethyl)-1-(5-ethoxy-5-oxopentyl)-2-methyl-1,2-hydrazindicarboxylat

isopropylamine

ethyl 5-bromovalerate

1-methyl-1,2-dicarbobenzoxy-hydrazine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 64377-83-9 dibenzyl 1-methyl-2-[5-oxo-5-(propan-2-ylamino)pentyl]hydrazine-1,2-dicarboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send