4-(Chlorocarbonyl)-2,6-difluoroanisole

Base Information

• Chemical Name: 4-(Chlorocarbonyl)-2,6-difluoroanisole
• CAS No.: 501701-43-5
• Molecular Formula: C8H5ClF2O2
• Molecular Weight: 206.576
• Hs Code.: 2918990090
• Mol file: 501701-43-5.mol

Synonyms:3.5-Difluor-p-anisidin;3,5-Difluor-4-methoxy-anilin;4-Amino-2,6-fluoroanisole;3,5-difluoro-4-methoxybenzenamine;3,5-difluoro-4-methoxy-benzoyl chloride;3,5-difluoro-4-methoxy-aniline;

Chemical Property of 4-(Chlorocarbonyl)-2,6-difluoroanisole

Chemical Property:

• PSA: 26.30000
• LogP: 2.35240

Purity/Quality:

99% ^*data from raw suppliers

3,5-Difluoro-4-methoxybenzoyl chloride 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(Chlorocarbonyl)-2,6-difluoroanisole

There total 4 articles about 4-(Chlorocarbonyl)-2,6-difluoroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-difluoro-4-methoxybenzoic acid (319-60-8) → 3,5-difluoro-4-methoxybenzoyl chloride (501701-43-5)

Guidance literature:

With thionyl chloride; In toluene; for 2h; Reflux;

Reference yield:

oxalyl dichloride (79-37-8) + 3,5-difluoro-4-methoxybenzoic acid (319-60-8) → 3,5-difluoro-4-methoxybenzoyl chloride (501701-43-5)

Guidance literature:

In chloroform; N,N-dimethyl-formamide;

Reference yield:

→ N-(4-chlorophenyl)-N-[(2S,4R)-1-(3,5-difluoro-4-methoxybenzoyl)-2-methyl-1,2,3,4-tetrahydroquinolin-4-yl]acetamide (868210-80-4) + 3,5-difluoro-4-methoxybenzoyl chloride (501701-43-5)

Guidance literature:

upstream raw materials:

3,5-difluoro-4-methoxybenzoic acid

oxalyl dichloride

Downstream raw materials:

N-(1,2-dimethylpropyl)-3,5-difluoro-4-methoxybenzamide

3-(3,5-difluoro-4-methoxybenzoyl)-2,3-dihydro-1,3-benzothiazole

3-(3,5-difluoro-4-methoxybenzoyl)-2,3-dihydro-1,1-dioxo-1,3-benzothiazole

3-(3,5-difluoro-4-hydroxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole

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