6-(3,3-DMA)chrysin

Base Information

• Chemical Name: 6-(3,3-DMA)chrysin
• CAS No.: 50678-91-6
• Molecular Formula: C20H18O4
• Molecular Weight: 322.361
• DSSTox Substance ID: DTXSID40332054
• Nikkaji Number: J1.496.152F
• Wikidata: Q27105567
• Metabolomics Workbench ID: 69651
• ChEMBL ID: CHEMBL163972
• Mol file: 50678-91-6.mol

Synonyms:6-prenylchrysin

Chemical Property of 6-(3,3-DMA)chrysin

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 322.12050905
• Heavy Atom Count: 24
• Complexity: 526

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=CCC1=C(C2=C(C=C1O)OC(=CC2=O)C3=CC=CC=C3)O)C

Technology Process of 6-(3,3-DMA)chrysin

There total 5 articles about 6-(3,3-DMA)chrysin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

5,7-dihydroxy-2-phenyl-chromen-4-one (480-40-0) + 3-methyl-2-buten-1-ol (556-82-1) → 6-Prenylchrysin (50678-91-6) + 8-Prenylchrysin (34125-75-2)

Guidance literature:

With zinc(II) chloride; In ethyl acetate; at 40 ℃; for 5h; Reflux;

DOI:10.3390/ijms22115472

Reference yield: 7.2%

5,7-dihydroxy-2-phenyl-chromen-4-one (480-40-0) + prenyl bromide (870-63-3) → 6-Prenylchrysin (50678-91-6) + 5,7-Dihydroxy-6,8-di-CC-prenylflavon (50678-89-2) + 8-Prenylchrysin (34125-75-2)

Guidance literature:

With tetraethylammonium iodide; In methanol; Irradiation;

DOI:10.1021/jm991128y

Reference yield:

2-methyl-3-buten-2-ol (115-18-4) + 5,7-dihydroxy-2-phenyl-chromen-4-one (480-40-0) → 6-Prenylchrysin (50678-91-6) + 8-Prenylchrysin (34125-75-2)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 50 ℃; for 12h;

DOI:10.3987/com-99-8827

upstream raw materials:

2-methyl-3-buten-2-ol

5,7-dihydroxy-2-phenyl-chromen-4-one

prenyl bromide

dimethylallyl diphosphate