(4-Methyl-2-nitrophenyl)hydrazine

Base Information

• Chemical Name: (4-Methyl-2-nitrophenyl)hydrazine
• CAS No.: 50707-83-0
• Molecular Formula: C7H9N3O2
• Molecular Weight: 167.167
• DSSTox Substance ID: DTXSID20396790
• Wikidata: Q82197694
• Mol file: 50707-83-0.mol

Synonyms:(4-methyl-2-nitrophenyl)hydrazine;50707-83-0;4-Methyl-2-nitrophenylhydrazine;Hydrazine, (4-methyl-2-nitrophenyl)-;SCHEMBL17546158;DTXSID20396790;COWMLQSNMSCSOL-UHFFFAOYSA-N;BBL020470;STK893176;AKOS004123514;1-(4-Methyl-2-nitrophenyl)hydrazine #;NCGC00335592-01;AB01328063-02

Chemical Property of (4-Methyl-2-nitrophenyl)hydrazine

Chemical Property:

• PSA: 83.87000
• LogP: 2.48530
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 167.069476538
• Heavy Atom Count: 12
• Complexity: 169

Purity/Quality:

1-(4-methyl-2-nitrophenyl)hydrazine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)NN)[N+](=O)[O-]

Technology Process of (4-Methyl-2-nitrophenyl)hydrazine

There total 4 articles about (4-Methyl-2-nitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N'-(4-methyl-2-nitro-phenyl)-hydrazidosulfuric acid (861512-43-8) → 4-Methyl-2-nitro-phenylhydrazin (50707-83-0)

Guidance literature:

With hydrogenchloride; at 80 ℃;

Reference yield:

4-methyl-2-nitroaniline (89-62-3) → 4-Methyl-2-nitro-phenylhydrazin (50707-83-0)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; sodium nitrite; Yield given. Multistep reaction; 1.) water, 0 deg C;

DOI:10.1039/P19800000982

Reference yield:

→ 4-Methyl-2-nitro-phenylhydrazin (50707-83-0)

Guidance literature:

With hydrogenchloride; tin(ll) chloride;

upstream raw materials:

N'-(4-methyl-2-nitro-phenyl)-hydrazidosulfuric acid

4-methyl-2-nitroaniline

Downstream raw materials:

N-acetyl-4-methyl-2-nitrophenylhydrazine

3,5-Dimethyl-1-(4-methyl-2-nitro-phenyl)-1H-pyrazole

C₁₄H₁₉N₃O₅

C₁₂H₁₆N₄O₄

Refernces

• 1、 Boido,Novelli,Savelli,Sparatore,Russo,Filippelli,Susanna,Marmo. "Preparation and pharmacologic activity of amido- derivatives of 3-methyl-3,4-dihydro benzo- and pyrido-1,2,4-triazin-3-acetic acids". . p. 279 - 301. Retrieved 2007/10/02.