2,3-Dimethyl-4-phenylfuran

Base Information

Chemical Name:2,3-Dimethyl-4-phenylfuran
CAS No.:5109-66-0
Molecular Formula:C12H12O
Molecular Weight:172.227
Hs Code.:
DSSTox Substance ID:DTXSID80518754
Nikkaji Number:J3.377.009J
Wikidata:Q82381563
Mol file:5109-66-0.mol

Synonyms:2,3-Dimethyl-4-phenylfuran;5109-66-0;2,3-dimethyl-4-phenyl furan;DTXSID80518754

Suppliers and Price of 2,3-Dimethyl-4-phenylfuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,3-Dimethyl-4-phenylfuran

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:172.088815002
Heavy Atom Count:13
Complexity:161

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(OC=C1C2=CC=CC=C2)C

Technology Process of 2,3-Dimethyl-4-phenylfuran

There total 4 articles about 2,3-Dimethyl-4-phenylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 70-11-1
α-bromoacetophenone

: 17795-76-5
3-Tributylstannanyl-butan-2-one

: 5109-66-0
2,3-Dimethyl-4-phenylfuran

Guidance literature:: In toluene; at 80 ℃; for 20h;
DOI:10.1039/c39830000989

Reference yield: 57.0%

: 3355-28-0
1-Bromo-2-butyne

: 70-11-1
α-bromoacetophenone

: 5109-66-0
2,3-Dimethyl-4-phenylfuran

Guidance literature:: 1-Bromo-2-butyne; α-bromoacetophenone; With indium; In tetrahydrofuran; water; at 20 ℃;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h;

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2014.06.107

Reference yield:

: 14920-89-9
2,3-dimethylfuran

: 591-50-4
iodobenzene

: 73186-37-5
2,3-dimethyl-5-phenylfuran

: 5109-66-0
2,3-Dimethyl-4-phenylfuran

Guidance literature:: With C₄₁H₃₆N₂O₅P₂Pd₂; silver carbonate; In toluene; at 120 ℃; for 15h; Overall yield = 10 %; regioselective reaction;
DOI:10.3987/COM-17-13824