Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-

Base Information

Chemical Name:Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-
CAS No.:518343-71-0
Molecular Formula:C13H17ISi
Molecular Weight:328.268
Hs Code.:
DSSTox Substance ID:DTXSID10477183
Wikidata:Q82309470
Mol file:518343-71-0.mol

Synonyms:Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-;518343-71-0;SCHEMBL13620854;DTXSID10477183

Suppliers and Price of Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:328.01442
Heavy Atom Count:15
Complexity:265

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=C(C=CC(=C1)C#C[Si](C)(C)C)I

Technology Process of Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl-

There total 3 articles about Silane, [(3-ethyl-4-iodophenyl)ethynyl]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 518342-63-7
2-ethyl-4-(trimethylsilylethynyl)aniline

: 518343-71-0
1-iodo-2-ethyl-4-[(trimethylsilyl)ethynyl]benzene

Guidance literature:: 2-ethyl-4-(trimethylsilylethynyl)aniline; With tert.-butylnitrite; boron trifluoride diethyl etherate; In diethyl ether; at -20 - 5 ℃;

With iodine; sodium iodide; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(02)01409-6

Reference yield:

: 99471-67-7
2-ethyl-4-iodo-phenylamine

: 518343-71-0
1-iodo-2-ethyl-4-[(trimethylsilyl)ethynyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Pd(PPh₃)2Cl₂; CuI; triethylamine / 20 °C

2.1: BF₃*Et₂O; t-BuONO / diethyl ether / -20 - 5 °C

2.2: 86 percent / NaI; I₂ / acetonitrile / 1 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tert.-butylnitrite; boron trifluoride diethyl etherate; triethylamine; In diethyl ether; 1.1: Sonogashira coupling;
DOI:10.1016/S0040-4020(02)01409-6

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 518343-71-0
1-iodo-2-ethyl-4-[(trimethylsilyl)ethynyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Pd(PPh₃)2Cl₂; CuI; triethylamine / 20 °C

2.1: BF₃*Et₂O; t-BuONO / diethyl ether / -20 - 5 °C

2.2: 86 percent / NaI; I₂ / acetonitrile / 1 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tert.-butylnitrite; boron trifluoride diethyl etherate; triethylamine; In diethyl ether; 1.1: Sonogashira coupling;
DOI:10.1016/S0040-4020(02)01409-6