3-Chloro-2-methyl-5-nitropyridine

Base Information

Chemical Name:3-Chloro-2-methyl-5-nitropyridine
CAS No.:51984-62-4
Molecular Formula:C6H5ClN2O2
Molecular Weight:172.56900
Hs Code.:2933399090
DSSTox Substance ID:DTXSID101299811
Mol file:51984-62-4.mol

Synonyms:3-CHLORO-2-METHYL-5-NITROPYRIDINE;51984-62-4;Pyridine, 3-chloro-2-methyl-5-nitro-;MFCD16556270;3-chloro-2-methyl-5-nitro-pyridine;SCHEMBL3345475;DTXSID101299811;2-Methyl-3-chloro-5-nitropyridine;BCA98462;AKOS022188274;DS-8894;SY242297;DB-193890;CS-0153532;EN300-6730802

Suppliers and Price of 3-Chloro-2-methyl-5-nitropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Chloro-2-Methyl-5-Nitropyridine
100mg
$ 60.00

Matrix Scientific
3-Chloro-2-methyl-5-nitropyridine 95%
10g
$ 2036.00

Crysdot
3-Chloro-2-methyl-5-nitropyridine 98%
25g
$ 593.00

Crysdot
3-Chloro-2-methyl-5-nitropyridine 98%
10g
$ 296.00

Chemenu
3-Chloro-2-methyl-5-nitropyridine 98%
10g
$ 280.00

Chemenu
3-Chloro-2-methyl-5-nitropyridine 98%
5g
$ 174.00

Chemenu
3-Chloro-2-methyl-5-nitropyridine 98%
25g
$ 560.00

Ambeed
3-Chloro-2-methyl-5-nitropyridine 98%
25g
$ 594.00

Ambeed
3-Chloro-2-methyl-5-nitropyridine 98%
10g
$ 297.00

Ambeed
3-Chloro-2-methyl-5-nitropyridine 98%
1g
$ 52.00

Total 11 raw suppliers

Chemical Property of 3-Chloro-2-methyl-5-nitropyridine

Chemical Property:

Boiling Point:248.7±35.0 °C(Predicted)
PKA:-0.37±0.20(Predicted)
PSA：58.71000
Density:1.406±0.06 g/cm3(Predicted)
LogP:2.47480
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:172.0039551
Heavy Atom Count:11
Complexity:159

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-2-Methyl-5-Nitropyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=N1)[N+](=O)[O-])Cl

Technology Process of 3-Chloro-2-methyl-5-nitropyridine

There total 2 articles about 3-Chloro-2-methyl-5-nitropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22353-40-8
2,3-dichloro-5-nitropyridine

: 13061-96-6
dihydroxy-methyl-borane

: 51984-62-4
3-chloro-2-methyl-5-nitropyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; at 100 ℃; for 6h;

Reference yield:

: 51984-62-4
3-chloro-2-methyl-5-nitropyridine

Guidance literature:: aus Aminopyridin 53a,NaNO2 u.HCl;
DOI:10.1021/jm00248a006

Reference yield:

: 51984-62-4
3-chloro-2-methyl-5-nitropyridine

: 51984-63-5
5-chloro-6-methyl-pyridin-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; ammonium chloride; water / methanol / 16 h / 20 °C

2: water; sodium nitrite; hydrogenchloride / 18 h / 0 - 70 °C

With hydrogenchloride; water; ammonium chloride; zinc; sodium nitrite; In methanol;