Ethyl (2E)-2-methyl-3-phenyl-2-butenoate

Base Information Edit

Chemical Name:Ethyl (2E)-2-methyl-3-phenyl-2-butenoate
CAS No.:52094-27-6
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:
DSSTox Substance ID:DTXSID201276301
Nikkaji Number:J1.050.726J,J3.277.401F
Mol file:52094-27-6.mol

Synonyms:52094-27-6;SCHEMBL21734206;DTXSID201276301;Ethyl (2E)-2-methyl-3-phenyl-2-butenoate

Suppliers and Price of Ethyl (2E)-2-methyl-3-phenyl-2-butenoate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl (2E)-2-methyl-3-phenyl-2-butenoate Edit

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:204.115029749
Heavy Atom Count:15
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=C(C)C1=CC=CC=C1)C
Isomeric SMILES:CCOC(=O)/C(=C(\C)/C1=CC=CC=C1)/C

Technology Process of Ethyl (2E)-2-methyl-3-phenyl-2-butenoate

There total 36 articles about Ethyl (2E)-2-methyl-3-phenyl-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 64-17-5
ethanol

: (E)-2-methyl-3-phenyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)but-2-enamide

: 52094-28-7,95102-89-9,52094-27-6
(E)-2-Methyl-3-phenyl-2-butensaeure-ethylester

Guidance literature:: With glycidyl methyl ether; potassium acetate; at 90 ℃; for 35h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.7b02841

Reference yield: 83.0%

: 1029612-60-9
(Z)-ethyl 3-(p-toluenesulfonyloxy)-2-methylbut-2-enoate

: phenylzinc pivalate

: 52094-28-7,95102-89-9,52094-27-6
(E)-2-Methyl-3-phenyl-2-butensaeure-ethylester

Guidance literature:: With [2,2]bipyridinyl; cobalt(II) bromide; In tetrahydrofuran; for 16h; Inert atmosphere;
DOI:10.1002/anie.201805486

Reference yield: 81.0%

: (E)-ethyl 2-methyl-3-(diphenoxyphosphoryloxy)but-2-enoate

: 98-80-6
phenylboronic acid

: 52094-28-7,95102-89-9,52094-27-6
(E)-2-Methyl-3-phenyl-2-butensaeure-ethylester

Guidance literature:: With [1,4-bis(diphenylphosphino)butane] palladium(ll) dichloride; sodium carbonate; In N,N-dimethyl-formamide; at 150 - 155 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c5ob01097g