Technology Process of Leucine, N-(phenylmethylene)-, 1,1-dimethylethyl ester
There total 1 articles about Leucine, N-(phenylmethylene)-, 1,1-dimethylethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
magnesium sulfate; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/jacs.7b05460
- Guidance literature:
-
α-methyl-γ-phenylallyl acetate; tert-butyl 2-(benzylideneamino)-4-methylpentanoate;
With
potassium phosphate; tetrakis(acetonitrile)copper(I)tetrafluoroborate; bis(η3-allyl-μ-chloropalladium(II)); 1-(bis(2-((R)-tert-butylsulfinyl)phenyl)phosphino)piperidine; (Rp,R)-tBu-FOXAP;
In
tetrahydrofuran;
at 10 ℃;
for 48h;
Inert atmosphere;
With
citric acid;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
stereoselective reaction;
Inert atmosphere;
DOI:10.1021/jacs.0c02150
- Guidance literature:
-
With
bis(η3-allyl-μ-chloropalladium(II)); C48H50FeN2O2P2; copper(II) bis(trifluoromethanesulfonate); caesium carbonate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
enantioselective reaction;
Inert atmosphere;
DOI:10.1021/jacs.7b05460
