5-Hexen-1-amine, N,N-dimethyl-

Base Information

• Chemical Name: 5-Hexen-1-amine, N,N-dimethyl-
• CAS No.: 52254-56-5
• Molecular Formula: C8H17N
• Molecular Weight: 127.23
• Mol file: 52254-56-5.mol

Synonyms:Hex-5-enyl-dimethyl-amin;Dimethyl-(δ-vinyl-butyl)-amin;1-Dimethylamino-hexen-(5);6-Dimethylamino-1-hexene;hex-5-enyl-dimethyl-amine;6-Dimethylamino-hexen-(1);

Chemical Property of 5-Hexen-1-amine, N,N-dimethyl-

Chemical Property:

• PSA: 3.24000
• LogP: 1.90430

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Hexen-1-amine, N,N-dimethyl-

There total 2 articles about 5-Hexen-1-amine, N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methylate (124-41-4) + dimethylhexahydroazepinium iodide (20422-15-5) → hexahydro-1-methyl-1H-azepine (1192-95-6) + 6-(dimethylamino)-1-methoxyhexane (58390-19-5) + N,N-dimethyhex-5-enylamine (52254-56-5)

Guidance literature:

In methanol; at 130 ℃; Rate constant;

DOI:10.1021/jo01308a002

Reference yield:

6-(N,N-dimethylamino)-1-hexanol (1862-07-3) → N,N-dimethyhex-5-enylamine (52254-56-5)

Guidance literature:

With aluminum oxide; at 287 ℃;

Reference yield:

N,N-dimethyhex-5-enylamine (52254-56-5) → 6-(N,N-dimethylamino)-1-hexanol (1862-07-3)

Guidance literature:

Multi-step reaction with 2 steps

1: BH₃-Et₃N / xylene / Heating

2: aq. NaOH, aq. H₂O₂ / tetrahydrofuran

With sodium hydroxide; triethylamine-borane; dihydrogen peroxide; In tetrahydrofuran; xylene;

upstream raw materials:

6-(N,N-dimethylamino)-1-hexanol

sodium methylate

dimethylhexahydroazepinium iodide

Downstream raw materials:

6-(N,N-dimethylamino)-1-hexanol