Silane, 1,3-benzodioxol-5-yltrimethyl-

Base Information

Chemical Name:Silane, 1,3-benzodioxol-5-yltrimethyl-
CAS No.:52287-50-0
Molecular Formula:C10H14O2Si
Molecular Weight:194.30200
Hs Code.:
DSSTox Substance ID:DTXSID70375378
Wikidata:Q82163909
Mol file:52287-50-0.mol

Synonyms:52287-50-0;1-(Trimethylsilyl)-3,4-(methylenedioxy)benzene;Silane, 1,3-benzodioxol-5-yltrimethyl-;1,3-benzodioxol-5-yl(trimethyl)silane;DTXSID70375378;AKOS006343314

Suppliers and Price of Silane, 1,3-benzodioxol-5-yltrimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
1-(TRIMETHYLSILYL)-3,4-(METHYLENEDIOXY)BENZENE
5g
$ 1943.00

Rieke Metals
1-(TRIMETHYLSILYL)-3,4-(METHYLENEDIOXY)BENZENE
1g
$ 809.00

Total 4 raw suppliers

Chemical Property of Silane, 1,3-benzodioxol-5-yltrimethyl-

Chemical Property:

PSA：18.46000
LogP:1.96050
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:194.076306220
Heavy Atom Count:13
Complexity:188

Purity/Quality:

99% ^*data from raw suppliers

1-(TRIMETHYLSILYL)-3,4-(METHYLENEDIOXY)BENZENE ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C1=CC2=C(C=C1)OCO2

Technology Process of Silane, 1,3-benzodioxol-5-yltrimethyl-

There total 5 articles about Silane, 1,3-benzodioxol-5-yltrimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-77-4
chloro-trimethyl-silane

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 52287-50-0
benzo[d][1,3]dioxol-5-yltrimethylsilane

Guidance literature:: 1,2-(methylenedioxy)-4-bromobenzene; With n-butyllithium; In tetrahydrofuran; n-Pentane; at -78 ℃; for 1h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; n-Pentane; at -78 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.orglett.2c00288

Reference yield: 71.0%

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: tris(trimethylsilyl)aluminum etherate

: 52287-50-0
benzo[d][1,3]dioxol-5-yltrimethylsilane

Guidance literature:: bis(triphenylphosphine)nickel(II) chloride; In 1,4-dioxane; for 1h; Heating;
DOI:10.1016/S0040-4039(01)99804-1

Reference yield: 65.0%

: 7228-38-8
5-chloro-1,3-benzodioxole

: sodium trimethylsilyldimethylsilanolate

: 52287-50-0
benzo[d][1,3]dioxol-5-yltrimethylsilane

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; Dimethyl(phenyl)phosphine; In toluene; at 70 ℃; for 18h; Schlenk technique; Sealed tube;
DOI:10.1039/d1cc02683f