2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine

Base Information

Chemical Name:2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine
CAS No.:22731-54-0
Molecular Formula:C21H15 Cl2 N
Molecular Weight:352.2565
Hs Code.:
NSC Number:202512
DSSTox Substance ID:DTXSID30308142
Mol file:22731-54-0.mol

Synonyms:22731-54-0;NSC202512;DTXSID30308142;NSC-202512;2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine

Suppliers and Price of 2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine

Chemical Property:

Vapor Pressure:3.63E-10mmHg at 25°C
Boiling Point:514°Cat760mmHg
Flash Point:264.7°C
Density:1.14g/cm³
XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:351.0581549
Heavy Atom Count:24
Complexity:421

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=C=C(C2=CC=C(C=C2)Cl)C3=CC=C(C=C3)Cl

Technology Process of 2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine

There total 5 articles about 2,2-Bis(4-chlorophenyl)-N-(4-methylphenyl)ethen-1-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68668-89-3
2,2-bis(4-chlorophenyl)acetyl chloride

: 2327-67-5
N-(p-tolyl)-P,P,P-triphenylphosphine imide

: 22731-54-0
2,2-bis(4-chlorophenyl)-N-(p-tolyl)ethen-1-imine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1039/c6cc05456k

Reference yield:

: 83-05-6
bis(4'-chlorophenyl)acetic acid

: 22731-54-0
2,2-bis(4-chlorophenyl)-N-(p-tolyl)ethen-1-imine

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

2: triethylamine / dichloromethane / 0.25 h / 20 °C

With oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c6cc05456k

Reference yield:

: 108-90-7
chlorobenzene

: 22731-54-0
2,2-bis(4-chlorophenyl)-N-(p-tolyl)ethen-1-imine

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / acetic acid / 80 °C / Cooling with ice

2: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

3: triethylamine / dichloromethane / 0.25 h / 20 °C

With oxalyl dichloride; sulfuric acid; triethylamine; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c6cc05456k