Benzoic acid, 4-methoxy-, 4-(chlorocarbonyl)phenyl ester

Base Information

Chemical Name:Benzoic acid, 4-methoxy-, 4-(chlorocarbonyl)phenyl ester
CAS No.:52899-54-4
Molecular Formula:C15H11ClO4
Molecular Weight:290.703
Hs Code.:
Mol file:52899-54-4.mol

Synonyms:4-[(4'-Methoxybenzoyl)oxy]benzoyl chloride;4-chloroformylphenyl-4-methoxybenzoate;Benzoic acid,4-methoxy-,4-(chlorocarbonyl)phenyl ester;

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Chemical Property of Benzoic acid, 4-methoxy-, 4-(chlorocarbonyl)phenyl ester

Chemical Property:

Boiling Point:438.0±30.0 °C(Predicted)
PSA：52.60000
Density:1.302±0.06 g/cm3(Predicted)
LogP:3.29340

Purity/Quality:

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Technology Process of Benzoic acid, 4-methoxy-, 4-(chlorocarbonyl)phenyl ester

There total 6 articles about Benzoic acid, 4-methoxy-, 4-(chlorocarbonyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 52899-69-1
4-(4'-methoxybenzoyloxy)benzoic acid

: 52899-54-4
4-[(4'-Methoxybenzoyl)oxy]benzoyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; Heating;
DOI:10.1080/00268948208071024

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 52899-54-4
4-[(4'-Methoxybenzoyl)oxy]benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Et₃N / CHCl₃ / 1 h / Ambient temperature

2: 57 percent / O₂ / cobalt bromide, manganese bromide / propionic acid / 12 h / Heating

3: 83 percent / SOCl₂, DMF / Heating

With thionyl chloride; oxygen; triethylamine; N,N-dimethyl-formamide; manganese(II) bromide; cobalt(II) bromide; In chloroform; propionic acid;
DOI:10.1080/00268948208071024

Reference yield:

: 56800-26-1
4-(4'-methoxybenzoyloxy)benzaldehyde

: 52899-54-4
4-[(4'-Methoxybenzoyl)oxy]benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / O₂ / cobalt bromide, manganese bromide / propionic acid / 12 h / Heating

2: 83 percent / SOCl₂, DMF / Heating

With thionyl chloride; oxygen; N,N-dimethyl-formamide; manganese(II) bromide; cobalt(II) bromide; In propionic acid;
DOI:10.1080/00268948208071024