5-Bromo-2,3-dihydroxybenzaldehyde

Base Information

Chemical Name:5-Bromo-2,3-dihydroxybenzaldehyde
CAS No.:52924-55-7
Molecular Formula:C7H5BrO3
Molecular Weight:217.019
Hs Code.:
DSSTox Substance ID:DTXSID10595134
Wikidata:Q82490078
Mol file:52924-55-7.mol

Synonyms:5-Bromo-2,3-dihydroxybenzaldehyde;52924-55-7;5-bromo-2,3-dihydroxy-benzaldehyde;SCHEMBL4062201;5bromo-2,3-dihydroxybenzaldehyde;DTXSID10595134;QOJBBGBTZFXYBV-UHFFFAOYSA-N;CCA92455;Benzaldehyde, 5-bromo-2,3-dihydroxy-;CS-0137210;E81705

Suppliers and Price of 5-Bromo-2,3-dihydroxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 5-Bromo-2,3-dihydroxybenzaldehyde

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:215.94221
Heavy Atom Count:11
Complexity:151

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1C=O)O)O)Br

Technology Process of 5-Bromo-2,3-dihydroxybenzaldehyde

There total 2 articles about 5-Bromo-2,3-dihydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5034-74-2
5-bromo-3-methoxysalicylaldehyde

: 52924-55-7
5-bromo-2,3-dihydroxybenzaldehyde

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 6h;
DOI:10.1021/jo050550l

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 52924-55-7
5-bromo-2,3-dihydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; potassium bromide; acetic acid / water / 2.42 h / 100 °C / Inert atmosphere; Large scale

2: acetic acid; water; hydrogen bromide / 39 h / 55 - 85 °C / 517.16 Torr / Inert atmosphere; Large scale

With water; hydrogen bromide; bromine; acetic acid; potassium bromide; In water;
DOI:10.1021/op034104g