2-bromo-5-methoxy-4-methylaniline

Base Information

• Chemical Name: 2-bromo-5-methoxy-4-methylaniline
• CAS No.: 532440-88-3
• Molecular Formula: C8H10BrNO
• Molecular Weight: 216.077
• Hs Code.: 2922290090
• Mol file: 532440-88-3.mol

Synonyms:Benzenamine, 2-bromo-5-methoxy-4-methyl-;2-Bromo-5-methoxy-4-methylbenzenamine;

Chemical Property of 2-bromo-5-methoxy-4-methylaniline

Chemical Property:

• Melting Point: 75-77°
• PSA: 35.25000
• LogP: 2.92950
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-5-methoxy-4-methylaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-bromo-5-methoxy-4-methylaniline

There total 2 articles about 2-bromo-5-methoxy-4-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ortho-cresidine (16452-01-0) → 2-bromo-5-methoxy-3-methylaniline (532440-88-3)

Guidance literature:

With tetra-N-butylammonium tribromide; In ethyl acetate; at 0 - 20 ℃;

DOI:10.1021/acs.jmedchem.6b01645

Reference yield: 85.0%

sodium hydrogencarbonate (144-55-8) + ortho-cresidine (16452-01-0) → 2-bromo-5-methoxy-3-methylaniline (532440-88-3)

Guidance literature:

With tetra-n-butylammonium tribromide; In hexane; dichloromethane; ethyl acetate;

Reference yield: 72.0%

zinc(II) cyanide (557-21-1) + 2-bromo-5-methoxy-3-methylaniline (532440-88-3) → 2-amino-4-methoxy-5-methylbenzonitrile

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h; Microwave irradiation;

DOI:10.1021/acs.jmedchem.6b01645

upstream raw materials:

sodium hydrogencarbonate

ortho-cresidine

Downstream raw materials:

2,4-dichloro-7-methoxy-6-methylquinazoline

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