4-{[(4-methoxyphenyl)carbothioyl]sulfanyl}butanoic acid

Base Information

• Chemical Name: 4-{[(4-methoxyphenyl)carbothioyl]sulfanyl}butanoic acid
• CAS No.: 36122-42-6
• Molecular Formula: C₁₂H₁₄O₃S₂
• Molecular Weight: 270.373
• Mol file: 36122-42-6.mol

Synonyms:NSC295581; p-Anisic acid, dithio-, ester with 4-mercaptobutyric acid

Chemical Property of 4-{[(4-methoxyphenyl)carbothioyl]sulfanyl}butanoic acid

Chemical Property:

• Vapor Pressure: 6.2E-09mmHg at 25°C
• Boiling Point: 451.3°C at 760 mmHg
• Flash Point: 226.8°C
• Density: 1.281g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-{[(4-methoxyphenyl)carbothioyl]sulfanyl}butanoic acid

There total 2 articles about 4-{[(4-methoxyphenyl)carbothioyl]sulfanyl}butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-butanolide (96-48-0) + carbon disulfide (75-15-0,12122-00-8) + 4-methoxyphenyl magnesium bromide (13139-86-1) → ω-Carboxypropyl-4-methoxydithiobenzoat (36122-42-6)

Guidance literature:

Multistep reaction; (i) THF, (ii) /BRN= 105248/;

Reference yield:

→ ω-Carboxypropyl-4-methoxydithiobenzoat (36122-42-6)

Guidance literature:

Dithiobenzoat II, alk. Hydrolyse;

DOI:10.1039/c39720000345

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + ω-Carboxypropyl-4-methoxydithiobenzoat (36122-42-6) → ω-Methoxycarbonyl-propyldithioester (36122-41-5)

Guidance literature:

upstream raw materials:

4-butanolide

carbon disulfide

4-methoxyphenyl magnesium bromide

Downstream raw materials:

ω-Methoxycarbonyl-propyldithioester

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