Benzene, (1-chloro-1-nitrosoethyl)-

Base Information

Chemical Name:Benzene, (1-chloro-1-nitrosoethyl)-
CAS No.:53441-57-9
Molecular Formula:C8H8ClNO
Molecular Weight:169.60800
Hs Code.:
Mol file:53441-57-9.mol

Synonyms:(1-chloro-1-nitroso-ethyl)-benzene;1-chloro-1-nitroso-1-phenylethane;Benzene,(1-chloro-1-nitrosoethyl);<1-Chlor-1-nitroso-ethyl>-benzol;(1-Chlor-1-nitroso-aethyl)-benzol;

Suppliers and Price of Benzene, (1-chloro-1-nitrosoethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (1-chloro-1-nitrosoethyl)-

Chemical Property:

Boiling Point:214-220 °C
PSA：29.43000
Density:1.14±0.1 g/cm3(Predicted)
LogP:2.86450

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, (1-chloro-1-nitrosoethyl)-

There total 4 articles about Benzene, (1-chloro-1-nitrosoethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 613-91-2
acetophenone oxime

: 2899-02-7,99515-28-3
N,N'-dichlorobis(2,4,6-trichlorodiphenyl)urea

: 53441-57-9
1-chloro-1-nitroso-1-phenylethane

: 20632-35-3
bis(2,4,6-trichlorodiphenyl)urea

Guidance literature:: In acetonitrile; at 20 ℃; for 0.583333h;
DOI:10.1016/j.tetlet.2006.12.001

Reference yield: 34.0%

: 613-91-2
acetophenone oxime

: 31657-66-6
1-chloro-1-nitro-1-phenylethane

: 53441-57-9
1-chloro-1-nitroso-1-phenylethane

Guidance literature:: With chloro-trimethyl-silane; nitro acetate; In dichloromethane; at -10 ℃;
DOI:10.1007/s12039-010-0091-y

Reference yield:

: 98-86-2
acetophenone

: 53441-57-9
1-chloro-1-nitroso-1-phenylethane

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrogen chloride; sodium carbonate / H₂O / pH 7 - 8

2: 95 percent / N-tert-butyl-N-chlorocyanamide / CCl₄ / 20 °C

With N-(tert-butyl)-N-chloro-cyanamide; hydroxylamine hydrochloride; sodium carbonate; In tetrachloromethane; water;
DOI:10.1016/j.tetlet.2005.09.131