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Acetophenone
Cas No: 98-86-2
No Data 25 Kilogram 200 Metric Ton/Month Jinan Yuewei Chemical Co.,Ltd Contact Supplier
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USD $ 6.5-6.5 / Metric Ton 1 Metric Ton 36 Metric Ton/Week Hangzhou Johoo Chemical Co., Ltd Contact Supplier
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Acetophenone CAS NO.98-86-2
Cas No: 98-86-2
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Cas No: 98-86-2
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Factory price Cosmetic ACETOPHENONE 98-86-2 Manufacturer
Cas No: 98-86-2
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
Acetophenone
Cas No: 98-86-2
No Data 1 Gram 1 Metric Ton/Week Henan Allgreen Chemical Co.,Ltd Contact Supplier
Acetophenone CAS#98-86-2
Cas No: 98-86-2
USD $ 2970.0-2970.0 / Kilogram 200 Kilogram 50 Metric Ton/Month ORCHID CHEMICAL SUPPLIES LTD Contact Supplier
Acetophenone
Cas No: 98-86-2
USD $ 2.0-3.0 / Kilogram 1 Kilogram 50 Metric Ton/Day EAST CHEMSOURCES LIMITED Contact Supplier

98-86-2 Usage

Safety Profile

Poison by intraperitoneal andsubcutaneous routes. Moderately toxic by ingestion. A skinand severe eye irritant. Mutation data reported. Narcotic inhigh concentration. A hypnotic. Flammable liquid. To fightfire, use foam, CO2, dry chemical. When heated
InChI:InChI=1/C8H8O/c1-7(9)8-5-3-2-4-6-8/h2-6H,1H3

98-86-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A12727)  Acetophenone, 99%    98-86-2 500ml 155.0CNY Detail
Alfa Aesar (A12727)  Acetophenone, 99%    98-86-2 2500ml 403.0CNY Detail
Alfa Aesar (A12727)  Acetophenone, 99%    98-86-2 10000ml 1420.0CNY Detail
Sigma-Aldrich (63634)  Acetophenone  TraceCERT®, certified reference material 98-86-2 63634-50MG 766.35CNY Detail
Sigma-Aldrich (00790)  Acetophenone  puriss. p.a., ≥99.0% (GC) 98-86-2 00790-250ML 769.86CNY Detail
Sigma-Aldrich (42163)  Acetophenone  analytical standard 98-86-2 42163-1ML-F 255.06CNY Detail
Sigma-Aldrich (42163)  Acetophenone  analytical standard 98-86-2 42163-5ML-F 993.33CNY Detail

98-86-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 20, 2017

Revision Date: Aug 20, 2017

1.Identification

1.1 GHS Product identifier

Product name acetophenone

1.2 Other means of identification

Product number -
Other names Ethanone,1-phenyl

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Acetophenone is used in perfumery as a fragrance ingredient in soaps, detergents, creams, lotions, and perfumes; as a flavoring agent in foods, nonalcoholic beverages, and tobacco; as a specialty solvent for plastics and resins; as a catalyst for the polymerization of olefins; and in organic syntheses as a photosensitizer.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:98-86-2 SDS

98-86-2Synthetic route

styrene
292638-84-7

styrene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N,N-dimethylpyrrolidinium formate; dihydrogen peroxide; palladium dichloride In water at 60℃; for 3h; Wacker oxidation;100%
With tert.-butylhydroperoxide; C21H19N5Pd(2+)*2BF4(1-) In decane; acetonitrile at 45℃; for 12h; Kinetics; Wacker Oxidation;100%
With water; oxygen In methanol; dimethyl sulfoxide at 80℃; under 1520.1 Torr; for 20h; Catalytic behavior; Reagent/catalyst; Solvent; Pressure; Wacker Oxidation; Autoclave;99%
1-chlorostyrene
618-34-8

1-chlorostyrene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With iron(III) chloride; air; water; 1,2-dichloro-ethane at 75℃; for 96h; regioselective reaction;100%
With hydrogenchloride
With sulfuric acid at 60℃;
ethylbenzene
100-41-4

ethylbenzene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With potassium permanganate; iron(III) chloride In acetone at -78 - 20℃; for 16h;100%
With potassium bromate; cerium(IV) oxide In 1,4-dioxane; water; acetic acid at 95℃; for 1h;100%
With cerium(IV) triflate; water In acetonitrile at 20℃; for 19.5h;99.7%
1-Phenylethanol
98-85-1, 13323-81-4

1-Phenylethanol

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With acetone; zirconic acid at 150℃;100%
With silica gel; copper(II) nitrate In tetrachloromethane for 0.25h; Zn(NO3)2;100%
With tetrakis(pyridine)silver dichromate In benzene for 0.5h; Heating;100%
rac-methylbenzylamine
618-36-0

rac-methylbenzylamine

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With 4-phenylnaphthalene-1,2-dione In acetonitrile at 80℃; Temperature; Reagent/catalyst;100%
With iodine; mercury(II) oxide In dichloromethane at 20℃; for 1h; Oxidation;98%
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; laccasefrom Trametes versicolor; oxygen In water at 30℃; pH=4.5; Enzymatic reaction;97%
acetyl chloride
75-36-5

acetyl chloride

benzene
71-43-2

benzene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation; Inert atmosphere;100%
With iron(III) oxide at 20℃; for 0.166667h; Friedel Crafts acylation; regioselective reaction;98%
With zinc at 60 - 62℃; for 0.00833333h; Friedel-Crafts acylation; microwave irradiation;95%
phenylacetylene
536-74-3

phenylacetylene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With mercuric triflate; water; tetramethylurea In dichloromethane; acetonitrile at 20℃; for 12h;100%
With Au nanoparticles covalently bonded to HS/SO3H functionalized periodic mesoporous organosilica (Et) at 70℃; for 1.5h; neat (no solvent);100%
With water at 59.84℃; for 24h; Ionic liquid;100%
isopropenylbenzene
98-83-9

isopropenylbenzene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With oxygen; 1,4-dimethoxybezene In acetonitrile for 12h; Mechanism; Ambient temperature; Irradiation; further substrates;100%
With dihydrogen peroxide In water at 75℃; for 6h;100%
With 1H-imidazole; sodium periodate; MnCl-TPP-(PEO750)4 In water; acetonitrile at 20℃; for 24h;99%
2-methyl-2-phenyl-[1,3]dithiane
6331-22-2

2-methyl-2-phenyl-[1,3]dithiane

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.5h; Micellar solution;100%
With silica gel; copper(II) nitrate In tetrachloromethane for 0.416667h; Ambient temperature;98%
With ammonium persulfate; Montmorillonite K-10 clay for 0.0333333h; microwave irradiation;98%
acetophenone oxime
613-91-2

acetophenone oxime

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With 2,2'-bipyridylchromium peroxide In benzene for 0.25h; Heating;100%
With 2,2'-bipyridylchromium peroxide In benzene for 0.25h; Product distribution; Heating; effect of various chromium(VI) based oxidants;100%
With 1-benzyl-4-aza-1-azoniabiyclo<2.2.2>octane peroxodisulfate In acetonitrile for 0.25h; Heating;100%
4-Iodoacetophenone
13329-40-3

4-Iodoacetophenone

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 36h; Inert atmosphere;100%
With triethylamine In toluene at 20℃; for 24h; Inert atmosphere; Irradiation; Sealed tube;83.4%
With tris-(trimethylsilyl)silane In acetonitrile Schlenk technique; Inert atmosphere; Irradiation;80%
iodoacetophenone
4636-16-2

iodoacetophenone

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; meso-5,10,15,20-tetraphenyl-21-monothiaporphyrin; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 22℃; for 18h; Irradiation;100%
With bismuth(III) chloride; sodium tetrahydroborate In tetrahydrofuran for 4h; Ambient temperature;94.2%
With indium; water for 3h; ultrasound;90%
2-Phenylpropanal
34713-70-7

2-Phenylpropanal

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 24h; Ambient temperature;100%
With sodium hydride In diethyl ether at 25℃; for 1h; Temperature; Reagent/catalyst;98%
With pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate In methanol at 25℃; under 1748 Torr;96.6%
acetophenonazine
729-43-1

acetophenonazine

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With 2-phenyl-1,2-benzoisoselenazol-3(2H)-one; dihydrogen peroxide In methanol; water at 20℃; for 48h;100%
With 2-phenyl-1,2-benzoisoselenazol-3(2H)-one; dihydrogen peroxide In methanol; water at 65℃; for 2h;100%
With dihydrogen peroxide; 2,2‘-diselenobis(N-phenylbenzamide) In methanol; water at 20℃; for 20h;100%
1-phenyl-1-trimethylsilyloxyethane
14856-75-8

1-phenyl-1-trimethylsilyloxyethane

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With benzyltriphenylphosphonium chlorate; aluminium trichloride In acetonitrile for 0.7h; Heating;100%
With nitrogen dioxide at 20℃; for 0.5h;100%
With bismuth(III) chloride; benzyltriphenylphosphonium peroxymonosulfate In dichloromethane for 0.05h; microwave irradiation;99%
α,β,β-trimethylstyrene
769-57-3

α,β,β-trimethylstyrene

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With sodium nitrite In water; acetic acid 1.) 0 deg C 2.) 60 deg C, 0,5 h;100%
acetophenone dimethyl acetal
4316-35-2

acetophenone dimethyl acetal

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With water; Nafion-H In acetone for 0.5h;100%
With Montmorillonite K10 In dichloromethane for 0.0833333h; Ambient temperature;100%
With water at 80℃; for 2h;100%
1,1,-diethoxy-1-phenylethane
4316-37-4

1,1,-diethoxy-1-phenylethane

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With water at 80℃; for 2h;100%
With sodium perborate In acetic acid at 25℃; for 0.5h;86%
perchloric acid In ethanol; water at 25 - 30℃; for 0.416667h;85%
With aluminium(III) iodide In acetonitrile; benzene for 0.166667h; Ambient temperature;86 % Chromat.
2,5-diphenyl-2,5-hexanediol
24434-16-0

2,5-diphenyl-2,5-hexanediol

A

Succinimide
123-56-8

Succinimide

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N-iodo-succinimide In benzene for 6h; Product distribution; Irradiation; varying reaction time;A 99%
B 100%
iodoacetophenone
4636-16-2

iodoacetophenone

Benzeneselenol
645-96-5

Benzeneselenol

A

diphenyl diselenide
1666-13-3

diphenyl diselenide

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With potassium carbonate In ethanol for 0.25h; Product distribution; Ambient temperature; other iodomethyl ketones;A 100%
B 100%
ethyl 3-oxo-3-phenylpropionate
94-02-0

ethyl 3-oxo-3-phenylpropionate

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With silver tetrafluoroborate; water In acetic acid at 110℃; for 10h; regioselective reaction;100%
In water; N,N-dimethyl-formamide at 160℃; for 0.05h; microwave irradiation;82%
With bis(cyclopentadienyl)titanium dichloride; isopropylmagnesium bromide In tetrahydrofuran; diethyl ether for 4h; Ambient temperature;63%
With magnesium chloride In dimethyl sulfoxide at 150℃; for 1h; Yield given;
Multi-step reaction with 2 steps
1.1: potassium hydroxide / water / 24.5 h / 20 °C
1.2: 0 °C
2.1: dichloromethane / 9 h / 25 °C
View Scheme
2,3,3-trimethyl-1-phenacylindoline
88920-01-8

2,3,3-trimethyl-1-phenacylindoline

A

2,3,3-trimethylindoleniune
1640-39-7

2,3,3-trimethylindoleniune

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
In diethyl ether for 2.75h; Irradiation;A 100%
B n/a
(1-bromoethyl)benzne
585-71-7, 38661-81-3

(1-bromoethyl)benzne

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With water; sodium hydroxide at 20℃; for 0.0833333h; Microwave irradiation;100%
With dihydrogen peroxide In ethanol for 1h; Heating;91%
With potassium chromate In dimethyl sulfoxide at 120℃; for 1h;90%
1-chloroacetophenone
532-27-4

1-chloroacetophenone

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With AcrH2; perchloric acid; tris(2,2’-bipyridine)ruthenium(II) In acetonitrile at 298℃; for 8h; Quantum yield; Mechanism; Irradiation; Electron-Transfer Rate Constants ;;100%
With AcrH2; perchloric acid; tris(2,2’-bipyridine)ruthenium(II) In acetonitrile at 298℃; for 8h; Irradiation;100%
With hydrogen iodide for 2h; Ambient temperature;100%
N-(1-phenylethylidene)phenylhydrazine
583-11-9, 59130-82-4

N-(1-phenylethylidene)phenylhydrazine

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With copper(II) sulfate In tetrahydrofuran; methanol; water for 2.5h; Heating;100%
With benzyltriphenylphosphonium dichromate In acetonitrile for 0.25h; Oxidation; Heating;98%
With benzyltriphenylphosphonium dichromate; silica gel for 0.0666667h;98%
α-bromoacetophenone
70-11-1

α-bromoacetophenone

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With AcrH2; perchloric acid; tris(2,2’-bipyridine)ruthenium(II) In acetonitrile at 298℃; for 7h; Irradiation;100%
With AcrH2; perchloric acid; tris(2,2’-bipyridine)ruthenium(II) In acetonitrile at 298℃; for 7h; Quantum yield; Mechanism; Irradiation; Electron-Transfer Rate Constants ; other conc. of HClO4;100%
With AcrD2; perchloric acid; tris(2,2’-bipyridine)ruthenium(II) In acetonitrile at 298℃; for 8h; Quantum yield; Irradiation;100%
cis-Octadecen-9-saeurephenacylester
90144-64-2

cis-Octadecen-9-saeurephenacylester

A

cis-Octadecenoic acid
112-80-1

cis-Octadecenoic acid

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-o-phenylenediamine In acetonitrile for 2h; Irradiation;A 100%
B n/a
mandelic acid-phenacyl ester
117356-19-1

mandelic acid-phenacyl ester

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N,N-dimethyl-aniline In acetonitrile for 2h; Irradiation;A 100%
B n/a
phenacyl 2-methoxyphenylacetate
132589-74-3

phenacyl 2-methoxyphenylacetate

A

2-methoxyphenylacetic acid
93-25-4

2-methoxyphenylacetic acid

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-o-phenylenediamine In acetonitrile for 2h; Irradiation;A 100%
B n/a
2-oxo-2-phenylethyl 2-(tert-butoxycarbonylamino)acetate
83316-95-4

2-oxo-2-phenylethyl 2-(tert-butoxycarbonylamino)acetate

A

BOC-glycine
4530-20-5

BOC-glycine

B

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-o-phenylenediamine In acetonitrile for 2h; Irradiation;A 100%
B n/a
benzaldehyde
100-52-7

benzaldehyde

acetophenone
98-86-2

acetophenone

benzalacetophenone
94-41-7

benzalacetophenone

Conditions
ConditionsYield
With sodium hydroxide In methanol Claisen-Schmidt Condensation; Reflux;100%
With sulfated TiO2 (5 wtpercent sulfate) for 0.0166667h; Microwave irradiation; Neat (no solvent);99.2%
With sulfated TiO2-P25 (Degussa titania) for 0.0166667h; Microwave irradiation; Neat (no solvent);99%
benzaldehyde
100-52-7

benzaldehyde

acetophenone
98-86-2

acetophenone

1,3-diphenyl-propen-3-one
614-47-1

1,3-diphenyl-propen-3-one

Conditions
ConditionsYield
With sodium hydroxide In methanol at 20℃; for 20h; Aldol Condensation;100%
With sodium hydroxide In ethanol at 20℃; for 48h; Claisen-Schmidt Condensation;99%
With sodium hydroxide In ethanol at 20℃; for 48h;99%
ethane-1,2-dithiol
540-63-6

ethane-1,2-dithiol

acetophenone
98-86-2

acetophenone

2-methyl-2-phenyl[1,3]dithiolane
5769-02-8

2-methyl-2-phenyl[1,3]dithiolane

Conditions
ConditionsYield
With perchloric acid; silica gel at 25 - 30℃; for 5h;100%
With toluene-4-sulfonic acid In benzene Heating;99%
With cobalt(II) bromide In dichloromethane for 1.25h; Ambient temperature;99%
bromoacetic acid methyl ester
96-32-2

bromoacetic acid methyl ester

acetophenone
98-86-2

acetophenone

(rac)-methyl 3-hydroxy-3-phenylbutanoate
91970-87-5

(rac)-methyl 3-hydroxy-3-phenylbutanoate

Conditions
ConditionsYield
With iodine; zinc In diethyl ether; benzene for 3h; Heating;100%
With samarium diiodide; mischmetall In tetrahydrofuran at 20℃; for 3.5h; Reformatsky reaction;54%
With zinc; benzene
Stage #1: acetophenone With cerium(III) chloride heptahydrate; zinc In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere;
Stage #2: bromoacetic acid methyl ester In tetrahydrofuran at 0 - 20℃; Inert atmosphere;
1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

acetophenone
98-86-2

acetophenone

acetophenone 1,1-dimethylhydrazone
28541-43-7

acetophenone 1,1-dimethylhydrazone

Conditions
ConditionsYield
With trifluoroacetic acid In benzene Reflux; Dean-Stark;100%
With acetic acid In methanol Reflux;60%
In methanol at 20℃;31%
allyl bromide
106-95-6

allyl bromide

acetophenone
98-86-2

acetophenone

2-phenylpent-4-en-2-ol
4743-74-2

2-phenylpent-4-en-2-ol

Conditions
ConditionsYield
With ammonium acetate; zinc In tetrahydrofuran at 0℃; for 0.0166667h; Barbier reaction;100%
With ammonium chloride; zinc In tetrahydrofuran; water at 20℃; for 0.166667h; sonication;99%
With 2,4,6-trimethyl-pyridine; chloro-trimethyl-silane; bis(cyclopentadienyl)titanium (III) chloride In tetrahydrofuran at 20℃; for 6h; Barbier type allylation; Inert atmosphere;99%
3-phenyl-propenal
104-55-2

3-phenyl-propenal

acetophenone
98-86-2

acetophenone

Conditions
ConditionsYield
Stage #1: acetophenone With sodium hydroxide In ethanol; water at 0 - 5℃;
Stage #2: 3-phenyl-propenal In ethanol; water
100%
With poly(N-vinylimidazole) In neat (no solvent) at 20℃; for 0.666667h; Aldol Condensation; Sonication; Green chemistry;92%
With sodium hydroxide In ethanol; water90%
4-Methylbenzyl alcohol
589-18-4

4-Methylbenzyl alcohol

acetophenone
98-86-2

acetophenone

1-phenyl-3-(4-tolyl)propan-1-one
1669-50-7

1-phenyl-3-(4-tolyl)propan-1-one

Conditions
ConditionsYield
With titanium(IV) oxide; potassium hydroxide In toluene at 100℃; for 10h; Sealed tube; Irradiation;100%
With potassium phosphate tribasic trihydrate; C39H32Cl2N5PRu In tert-Amyl alcohol at 120℃; for 4h; Inert atmosphere; Schlenk technique;94%
With dimanganese decacarbonyl; sodium hydroxide In toluene at 110℃; for 2h; Inert atmosphere; Glovebox; Sealed tube;94%
potassium cyanide
151-50-8

potassium cyanide

acetophenone
98-86-2

acetophenone

2-hydroxy-2-phenylpropionitrile
20102-12-9

2-hydroxy-2-phenylpropionitrile

Conditions
ConditionsYield
Stage #1: potassium cyanide; acetophenone With 18-crown-6 ether In dichloromethane at 20℃; for 4h;
Stage #2: With hydrogenchloride In tetrahydrofuran; dichloromethane at 0 - 20℃; for 2h;
100%
Stage #1: potassium cyanide; acetophenone With tetrachlorosilane In acetonitrile at 60 - 70℃; for 5h;
Stage #2: With sodium hydrogencarbonate In water; acetonitrile Further stages.;
82%
With hydrogenchloride
acetophenone
98-86-2

acetophenone

para-Chlorobenzyl alcohol
873-76-7

para-Chlorobenzyl alcohol

3-(4-chlorophenyl)-1-phenylpropan-1-one
5739-39-9

3-(4-chlorophenyl)-1-phenylpropan-1-one

Conditions
ConditionsYield
With titanium(IV) oxide; potassium hydroxide In toluene at 100℃; for 10h; Sealed tube; Irradiation;100%
With C27H24Cl3F6IrN2; potassium hydroxide In toluene at 130℃; for 2h;94%
With C16H14IrN2O3; caesium carbonate In tert-Amyl alcohol for 6h; Reflux;91%
acetophenone
98-86-2

acetophenone

methylamine
74-89-5

methylamine

N-(1-phenylethylidene)methanamine
6907-71-7

N-(1-phenylethylidene)methanamine

Conditions
ConditionsYield
In ethanol at 20℃; for 48h; Molecular sieve; Inert atmosphere;100%
In ethanol at 20℃; for 48h; Molecular sieve; Inert atmosphere;100%
With triethylamine In ethanol for 1h; Molecular sieve;97%
acetophenone
98-86-2

acetophenone

2-hydroxyethanethiol
60-24-2

2-hydroxyethanethiol

2-methyl-2-phenyl-[1,3]oxathiolane
5684-32-2

2-methyl-2-phenyl-[1,3]oxathiolane

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In diethyl ether for 3h; Heating;100%
With tantalum pentachloride In dichloromethane at 20℃; for 1h;93%
With scandium tris(trifluoromethanesulfonate) In dichloromethane at 20℃; for 10h;90%
acetophenone
98-86-2

acetophenone

malononitrile
109-77-3

malononitrile

2-(1-phenylethylidene)propanedinitrile
5447-87-0

2-(1-phenylethylidene)propanedinitrile

Conditions
ConditionsYield
With ethylenediamine-modified poly(vinyl chloride) at 20℃; for 0.116667h; Solvent; Knoevenagel Condensation; Green chemistry;100%
With third generation polystyrene supported poly(amidoamine) dendrimer In ethanol at 50℃; for 0.5h; Knoevenagel condensation;98%
With MIL-53(Fe) metal organic framework encapsulated on silica-coated nickel ferrite magnetic nanoparticles In ethanol at 20℃; for 2h; Knoevenagel Condensation;95%
acetophenone
98-86-2

acetophenone

ethylhydrazine carboxylate
4114-31-2

ethylhydrazine carboxylate

N-ethoxycarbonyl-N'-(1-phenyl-ethylidene)-hydrazine
25445-76-5

N-ethoxycarbonyl-N'-(1-phenyl-ethylidene)-hydrazine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
With toluene-4-sulfonic acid In benzene for 4h; Heating;100%
100%
acetophenone
98-86-2

acetophenone

benzylmagnesium chloride
6921-34-2

benzylmagnesium chloride

1,2-diphenylpropane-2-ol
5342-87-0

1,2-diphenylpropane-2-ol

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃;100%
acetophenone
98-86-2

acetophenone

trimethyl orthoformate
149-73-5

trimethyl orthoformate

acetophenone dimethyl acetal
4316-35-2

acetophenone dimethyl acetal

Conditions
ConditionsYield
With toluene-4-sulfonic acid In methanol Heating;100%
With lithium tetrafluoroborate In methanol for 5h; Heating;99%
With cerium triflate In methanol at 20℃; for 0.5h;98%
acetophenone
98-86-2

acetophenone

acetophenone oxime
613-91-2

acetophenone oxime

Conditions
ConditionsYield
With acetic acid; acetone oxime at 125℃; for 2h;100%
With hydroxylamine hydrochloride100%
With hydroxylamine hydrochloride In acetonitrile at 70 - 110℃; for 15h; Solvent; Temperature; Time; chemoselective reaction;100%
acetophenone
98-86-2

acetophenone

2,3-diphenyl-2,3-butanediol
1636-34-6

2,3-diphenyl-2,3-butanediol

Conditions
ConditionsYield
With naphthalene; lithium; manganese(ll) chloride In tetrahydrofuran at 20℃; for 20h;100%
With tris(4,4'-dimethyl-2,2'bipyridine)ruthenium(II) ion; ascorbate In water for 3h; pH=12.7; Irradiation;100%
With samarium In acetonitrile at 20℃; for 0.5h;99%
acetophenone
98-86-2

acetophenone

ethylbenzene
100-41-4

ethylbenzene

Conditions
ConditionsYield
With hydrogen at 80℃; under 37503.8 Torr; for 0.5h; Autoclave; chemoselective reaction;100%
With hydrogen In ethanol at 39.84℃; under 760.051 Torr; for 5h;100%
With Pd/C; hydrogen In chloroform at 20℃; under 760.051 Torr; for 8h; Catalytic behavior;100%
acetophenone
98-86-2

acetophenone

1-Phenylethanol
98-85-1, 13323-81-4

1-Phenylethanol

Conditions
ConditionsYield
palladium on activated charcoal at 20℃; electrohydrogenation in 1 N aqeous-alcoholic NaOH;100%
With potassium hydroxide; BF4; isopropyl alcohol at 65℃; for 24h; Product distribution; variation of catalyst and reaction parameters; also with chiral complex catalyst;100%
With Triethoxysilane; cesium fluoride at 25℃; for 0.016h;100%
acetophenone
98-86-2

acetophenone

(S)-1-phenylethanol
1445-91-6

(S)-1-phenylethanol

Conditions
ConditionsYield
With carrot (Daucus carota, root); chloramphenicol In ethanol; water at 25℃; for 72h;100%
With Daucus carota root cells; chloramphenicol In water; dimethyl sulfoxide at 25℃; for 24h;100%
With borane-dimethyl sulfide complex; methyl 2-(5-chloro-2-hydroxybenzylamino)-3-methylbutanoate In tetrahydrofuran at 65℃; optical yield given as %ee; enantioselective reaction;100%
acetophenone
98-86-2

acetophenone

Acetophenone-methyl-d3
17537-31-4

Acetophenone-methyl-d3

Conditions
ConditionsYield
With 4 A molecular sieve; water-d2 at 180℃; under 9000.72 Torr; for 0.5h; microwave irradiation;100%
With pyrrolidine; water-d2 In 1,4-dioxane at 20℃; for 12h; Reagent/catalyst; Solvent;96%
With water-d2; potassium carbonate In 1,4-dioxane for 48h; Heating;93%
acetophenone
98-86-2

acetophenone

rac-1-cyclohexylethanol
1193-81-3

rac-1-cyclohexylethanol

Conditions
ConditionsYield
With hydrogen In water at 100℃; under 15001.5 Torr; for 0.333333h;100%
With ruthenium nanoparticles at 120℃; under 90009 Torr; for 2h; Ionic liquid; Autoclave;99%
With ruthenium; hydrogen In water at 30℃; under 22801.5 Torr; for 12h; Autoclave;94%
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