9-bromononyl Acetate

Base Information

• Chemical Name: 9-bromononyl Acetate
• CAS No.: 53596-82-0
• Molecular Formula: C11H21BrO2
• Molecular Weight: 265.191
• Nikkaji Number: J1.769.428F
• Mol file: 53596-82-0.mol

Synonyms:9-bromononyl Acetate;9-broMo-1-nonanol acetate;53596-82-0;SCHEMBL535694

Chemical Property of 9-bromononyl Acetate

Chemical Property:

• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 10
• Exact Mass: 264.07249
• Heavy Atom Count: 14
• Complexity: 137

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCCCCCCCCCBr

Technology Process of 9-bromononyl Acetate

There total 2 articles about 9-bromononyl Acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

9-bromononan-1-ol (55362-80-6) + acetic anhydride (108-24-7) → 9-bromononyl acetate (53596-82-0)

Guidance literature:

zinc(II) perchlorate; at 20 ℃; for 0.333333h;

DOI:10.1002/ejoc.200300458

Reference yield:

1,9-Dibromononane (4549-33-1) + potassium acetate (127-08-2) → 9-bromononyl acetate (53596-82-0) + 1,9-nonanediol diacetate (4944-60-9)

Guidance literature:

With acetic anhydride; acetic acid; at 125 - 140 ℃;

Reference yield: 92.0%

9-bromononyl acetate (53596-82-0) → 9-bromononan-1-ol (55362-80-6)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; for 1.5h; Heating;

DOI:10.1002/anie.199723441

upstream raw materials:

1,9-Dibromononane

potassium acetate

9-bromononan-1-ol

acetic anhydride

Downstream raw materials:

non-8-en-1-ol

(9-Acetoxynonyl)-triphenylphosphonium-bromid

9-bromononan-1-ol

non-8-en-1-yl acetate

Refernces

• 1、 -. "REDOX MOLECULES AND METHODS OF MAKING THE SAME". Page/Page column 11-12. . Retrieved 2010/12/29.
• 2、 Bartoli, Giuseppe,Bosco, Marcella,Dalpozzo, Renato,Marcantoni, Enrico,Massaccesi, Massimo,Rinaldi, Samuele,Sambri, Letizia. "Mg(ClO4)2 as a powerful catalyst for the acylation of alcohols under solvent-free conditions". . p. 39 - 42. Retrieved 2007/10/03.