1,9-NONANEDIOL DIACETATE

Base Information

• Chemical Name: 1,9-NONANEDIOL DIACETATE
• CAS No.: 4944-60-9
• Molecular Formula: C13H24O4
• Molecular Weight: 244.331
• Hs Code.: 2915390090
• Mol file: 4944-60-9.mol

Synonyms:1,9-Nonanediol,diacetate (6CI,7CI,8CI,9CI);NSC 53803;1,9-Diacetoxynonane;

Chemical Property of 1,9-NONANEDIOL DIACETATE

Chemical Property:

• Refractive Index: 1.4350-1.4380
• Boiling Point: 287.7 °C at 760 mmHg
• Flash Point: 129.2 °C
• PSA: 52.60000
• Density: 0.976 g/cm³
• LogP: 2.84330
• Storage Temp.: Refrigerator, Under inert atmosphere
• Solubility.: Chloroform (Slightly), Hexane (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,9-Diacetoxynonane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1,9-Diacetoxynonane is useful in polymeric-based coatings for improved tribological performance.

Technology Process of 1,9-NONANEDIOL DIACETATE

There total 7 articles about 1,9-NONANEDIOL DIACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol (98847-00-8) + acetic acid (64-19-7,77671-22-8) → 1,9-nonanediol diacetate (4944-60-9)

Guidance literature:

With iron(III) chloride; at 20 ℃; for 1h;

DOI:10.1055/s-1999-2806

Reference yield: 72.0%

1,9-Nonanediol (3937-56-2) + acetic acid (64-19-7,77671-22-8) → 9-hydroxyl nonanyl acetate (103109-24-6) + 1,9-nonanediol diacetate (4944-60-9)

Guidance literature:

With sulfuric acid; In water; for 44h;

DOI:10.1080/00397910801929341

Reference yield:

1,9-Nonanediol (3937-56-2) + acetyl chloride (75-36-5) → 1,9-nonanediol diacetate (4944-60-9)

Guidance literature:

With diethyl ether;

DOI:10.1021/ja01526a072

upstream raw materials:

1,9-Dibromononane

potassium acetate

1,9-Nonanediol

acetic anhydride

Downstream raw materials:

nona-1,8-diene

non-8-en-1-yl acetate

Refernces

• 1、 Hornyanszky, Gabor,Rohaly, Janos,Novak, Lajos. "Facile synthesis of mill moth's sex pheromone components". . p. 1533 - 1540. Retrieved 2008/09/20.
• 2、 Sharma,Mahalingam,Nagarajan,Ilangovan,Radhakrishna, Palakodety. "Facile acetylation of alcohols, ethers and ketals with catalytic FeCl3 in AcOH". . p. 1200 - 1202. Retrieved 2007/10/03.