3'-METHOXYFLAVONE

Base Information

• Chemical Name: 3'-METHOXYFLAVONE
• CAS No.: 53906-83-5
• Molecular Formula: C16H12O3
• Molecular Weight: 252.269
• Mol file: 53906-83-5.mol

Synonyms:2-(3-Methoxy-phenyl)-chromen-4-on;2-(3-methoxy-phenyl)-chromen-4-one;2-(3-methoxyphenyl)-4H-chromen-4-one;3'-Methoxy-flavon;3'-Methoxy-flavone;

Chemical Property of 3'-METHOXYFLAVONE

Chemical Property:

• Vapor Pressure: 6.25E-07mmHg at 25°C
• Boiling Point: 410oC at 760 mmHg
• Flash Point: 193.4oC
• PSA: 39.44000
• Density: 1.24g/cm3
• LogP: 3.46860

Purity/Quality:

3-Methoxyflavone 99% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-METHOXYFLAVONE

There total 40 articles about 3'-METHOXYFLAVONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,3-dihydro-2-(3-methoxyphenyl)-4H-1-benzopyran-4-one (67765-54-2,93514-38-6,127179-85-5) → 3'-methoxyflavone (53906-83-5)

Guidance literature:

With pyrrolidone hydrotribromide; In dimethyl sulfoxide; at 80 ℃; for 2h;

DOI:10.1246/bcsj.58.1599

Reference yield: 94.0%

2'-hydroxy-3-methoxy-chalcone (34000-28-7,7146-86-3) → 3'-methoxyflavone (53906-83-5)

Guidance literature:

With cerium (IV) sulfate tetrahydrate; silica gel; In neat (no solvent); at 100 ℃; for 4h; Green chemistry;

DOI:10.1080/00397911.2016.1230217

Reference yield: 94.0%

1-(2-hydroxyphenyl)-3-(3-methoxyphenyl)-1,3-propanedione (84634-65-1) → 3'-methoxyflavone (53906-83-5)

Guidance literature:

With iron(III) chloride; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1515/HC.2005.11.1.97

upstream raw materials:

2'-hydroxy-3-methoxy-chalcone

3-methoxy-2'-hydroxychalcone

2,3-dihydro-2-(3-methoxyphenyl)-4H-1-benzopyran-4-one

2-(3-methoxyphenyl)-2H-chromene

Downstream raw materials:

3'-hydroxyflavone

(+)-2-(3-methoxyphenyl)chroman-4-one

2,3-dihydro-2-(3-methoxyphenyl)-4H-1-benzopyran-4-one

C₂₂H₁₆N₄O₆

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