2(5H)-Furanone, 4-butyl-

Base Information

Chemical Name:2(5H)-Furanone, 4-butyl-
CAS No.:54145-06-1
Molecular Formula:C8H12O2
Molecular Weight:140.182
Hs Code.:
DSSTox Substance ID:DTXSID00467154
Nikkaji Number:J1.952.595C
Wikidata:Q82293960

Synonyms:2(5H)-Furanone, 4-butyl-;54145-06-1;3-butyl-2H-furan-5-one;DTXSID00467154;4-Butyl-2,5-dihydrofuran-2-one

Suppliers and Price of 2(5H)-Furanone, 4-butyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2(5H)-Furanone, 4-butyl-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:140.083729621
Heavy Atom Count:10
Complexity:159

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1=CC(=O)OC1

Technology Process of 2(5H)-Furanone, 4-butyl-

There total 1 articles about 2(5H)-Furanone, 4-butyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 201230-82-2
carbon monoxide

: 693-02-7
hex-1-yne

: 100378-66-3
3-n-butylmaleic anhydride

: 2035-76-9
3-butyldihydrofuran-2,5-dione

: 54145-06-1
4-n-butyl-2(5H)furan-2-one

: 71725-42-3
3-n-butyl-2(5H)-furanone

Guidance literature:: With water; potassium iodide; palladium(II) iodide; In 1,4-dioxane; at 80 ℃; for 15h; under 7600 Torr;
DOI:10.1016/S0040-4039(98)02464-2

Reference yield:

: 54145-06-1
4-n-butyl-2(5H)furan-2-one

: 4α-butyl-3α-(2α-phenylcyclopropyl)-dihydrofuran-2-one

: 4α-butyl-3α-(2α-phenylcyclopropyl)-dihydrofuran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.3: 16 h / 20 °C / Inert atmosphere

3.1: rhodium(II) pivalate / hexane / 1 h / -50 °C / Inert atmosphere

With rhodium(II) pivalate; palladium 10% on activated carbon; hydrogen; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; ethyl acetate;
DOI:10.1021/ja3046712