1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-

Base Information

Chemical Name:1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-
CAS No.:54161-63-6
Molecular Formula:C15H13N3O
Molecular Weight:251.288
Hs Code.:
DSSTox Substance ID:DTXSID10351075

Synonyms:54161-63-6;CDS1_000901;1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-;Maybridge1_005653;Oprea1_156987;DivK1c_001941;DTXSID10351075

Suppliers and Price of 1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:251.105862047
Heavy Atom Count:19
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=NC2=NC3=CC=CC=C3N2

Technology Process of 1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]-

There total 2 articles about 1H-Benzimidazol-2-amine, N-[(4-methoxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 934-32-7
1H-benzimidazol-2-amine

: 123-11-5
4-methoxy-benzaldehyde

: 54161-63-6
N-(4-methoxybenzylidene)-1H-benzo[d]imidazol-2-amine

Guidance literature:: With bismuth(III) chloride; In methanol; for 0.00694444h; Microwave irradiation;
DOI:10.13005/ojc/280175

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 54161-63-6
N-(4-methoxybenzylidene)-1H-benzo[d]imidazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile; water; methanol / 12 h / 20 °C

2: toluene / 24 h / 130 °C / Dean-Stark

In methanol; water; toluene; acetonitrile;
DOI:10.2174/1573406411309030017

Reference yield: 83.0%

: 1217-89-6
1-benzylisatin

: 54161-63-6
N-(4-methoxybenzylidene)-1H-benzo[d]imidazol-2-amine

: (R)-1'-benzyl-2-(4-methoxyphenyl)spiro[benzo[4,5]imidazo[1,2-c][1,3,5]oxadiazine-4,3'-indolin]-2'-one

Guidance literature:: With 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; C₁₈H₁₂BrCl₃N₃O⁽¹⁺⁾*BF₄^(1-); N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 48h; enantioselective reaction;
DOI:10.1002/anie.202016506