2-(4-Methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole

Base Information

• Chemical Name: 2-(4-Methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole
• CAS No.: 5819-30-7
• Molecular Formula: 2C₇H₄NO₄*Cu
• Molecular Weight: 395.772
• DSSTox Substance ID: DTXSID50386745

Synonyms:5819-30-7;2-(4-methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole;ST009328;CBMicro_049294;DTXSID50386745;4-methoxy-1-(5-phenyl(1,3,4-thiadiazolin-2-yl))naphthalene;AKOS024274957;BIM-0049350.P001

Chemical Property of 2-(4-Methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole

Chemical Property:

• Vapor Pressure: 1.86E-10mmHg at 25°C
• Boiling Point: 508.4°Cat760mmHg
• Flash Point: 261.3°C
• Density: 1.26g/cm³
• XLogP3: 5.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 320.09833431
• Heavy Atom Count: 23
• Complexity: 435

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C2=CC=CC=C21)C3NN=C(S3)C4=CC=CC=C4

Technology Process of 2-(4-Methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole

There total 3 articles about 2-(4-Methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-nitrobenzoic acid (552-16-9,104810-18-6) + copper dichloride → copper(II) 2-nitrobenzoate (5819-30-7,27269-44-9)

Guidance literature:

With NaOH; In water; acetone; neutralization of nitrobenzoic acid soln. (acetone) by aq. NaOH soln., addn. of small excess of acid, filtration, addn. of filtrate to aq. metal chloride soln., stirring (0.5 h); filtration, washing (water), drying (air, than vac. 140°C, 4 h);

DOI:10.1016/S0277-5387(00)80303-4

Reference yield:

copper(II) sulfate (7758-99-8) + potassium o-nitrobenzoate (15163-59-4) → copper(II) 2-nitrobenzoate (5819-30-7,27269-44-9)

Guidance literature:

In water; concd. soln.; equivalent amounts;;

Reference yield:

ammonium o-nitrobenzoate (19328-55-3) + copper(II) sulfate (7758-99-8) → copper(II) 2-nitrobenzoate (5819-30-7,27269-44-9)

Guidance literature:

In water; concd. soln.; equivalent amounts;;

upstream raw materials:

ortho-nitrobenzoic acid

copper(II) sulfate

potassium o-nitrobenzoate

ammonium o-nitrobenzoate

Downstream raw materials:

Cu(2-O₂NC₆H₄COO)2(1-phenylpiperazine)2

Cu(2-O₂NC₆H₄COO)2(4-methylpiperidine)2

Cu(2-O₂NC₆H₄COO)2(3-methylpiperidine)2

bis(2-amino-2-methyl-1-propanol)bis(o-nitrobenzoato-O)copper(II)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 5819-30-7 2-(4-methoxynaphthalen-1-yl)-5-phenyl-2,3-dihydro-1,3,4-thiadiazole

Send

Send

Metric Ton KG G Pound L ML

Send

Send