1-Azido-2-iodobenzene

Base Information

Chemical Name:1-Azido-2-iodobenzene
CAS No.:54467-95-7
Molecular Formula:C6H4IN3
Molecular Weight:245.022
Hs Code.:2929909090
European Community (EC) Number:684-472-9
DSSTox Substance ID:DTXSID10508466
Nikkaji Number:J1.730.885H
Wikidata:Q82365408
Mol file:54467-95-7.mol

Synonyms:1-azido-2-iodobenzene;54467-95-7;azidoiodobenzene;SCHEMBL13816909;DTXSID10508466;AKOS009323298;EN300-271760;1-Azido-2-iodobenzene 0.5 M in tert-butyl methyl ether

Suppliers and Price of 1-Azido-2-iodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
1-Azido-2-iodobenzene
5g
$ 3032.00

AK Scientific
1-Azido-2-iodobenzene
2.5g
$ 2092.00

Total 3 raw suppliers

Chemical Property of 1-Azido-2-iodobenzene

Chemical Property:

Refractive Index:1.6631
Boiling Point:90-91 °C(Press: 0.9 Torr)
PSA：49.75000
Density:1.8893
LogP:2.68576
Storage Temp.:?20°C
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:244.94499
Heavy Atom Count:10
Complexity:153

Purity/Quality:

99% ^*data from raw suppliers

1-Azido-2-iodobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,T
Statements: 11-38-48/23/24/25
Safety Statements: 16

MSDS Files:: Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC=C(C(=C1)N=[N+]=[N-])I

Technology Process of 1-Azido-2-iodobenzene

There total 11 articles about 1-Azido-2-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 615-43-0
2-iodophenylamine

: 54467-95-7
1-azido-2-iodo-benzene

Guidance literature:: 2-iodophenylamine; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; Inert atmosphere; Schlenk technique;

With sodium azide; In water; at 0 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/C8OB01837E

Reference yield: 80.0%

: 250160-25-9
N,N-tetramethylene-N'-(2'-iodophenyl)triazene

: 54467-95-7
1-azido-2-iodo-benzene

Guidance literature:: With sodium azide; boron trifluoride diethyl etherate; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/jo070774z

Reference yield: 73.0%

: 1005-07-8
o-azidoaniline

: 54467-95-7
1-azido-2-iodo-benzene

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 5 - 20 ℃; for 0.666667h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ja3089907