1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone

Base Information

Chemical Name:1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone
CAS No.:54730-26-6
Molecular Formula:C15H20O4
Molecular Weight:264.321
Hs Code.:
DSSTox Substance ID:DTXSID901148620
Nikkaji Number:J1.112.170E

Synonyms:DTXSID901148620;54730-26-6;1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone

Suppliers and Price of 1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:264.13615911
Heavy Atom Count:19
Complexity:320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCC1=C(C=CC(=C1O)C(=O)C)OCOC)C

Technology Process of 1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone

There total 7 articles about 1-[2-Hydroxy-4-(methoxymethoxy)-3-(3-methyl-2-buten-1-yl)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 19825-40-2
2,4-Dihydroxy-3-C-prenylacetophenone

: 107-30-2
chloromethyl methyl ether

: 54730-26-6
4-methoxymethoxy-3-(3,3-dimethylallyl)-2-hydroxyacetophenone

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 2h;
DOI:10.1002/ardp.200700057

Reference yield:

: 1314539-20-2
2'-prenyloxy-4'-methoxymethoxyacetophenone

: 54730-26-6
4-methoxymethoxy-3-(3,3-dimethylallyl)-2-hydroxyacetophenone

Guidance literature:: With activated clay; In dichloromethane; for 1.5h; Cooling with ice;

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 54730-26-6
4-methoxymethoxy-3-(3,3-dimethylallyl)-2-hydroxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaOH / acetone

1.2: acetone; benzene / Heating

2.1: 70 percent / K₂CO₃ / acetone / 2 h / 20 °C

With sodium hydroxide; potassium carbonate; In acetone;
DOI:10.1002/ardp.200700057