3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide

Base Information

Chemical Name:3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide
CAS No.:54754-75-5
Molecular Formula:C7H7BrN2O3
Molecular Weight:247.048
Hs Code.:
DSSTox Substance ID:DTXSID20514679
Wikidata:Q82375154

Synonyms:54754-75-5;3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide;DTXSID20514679;AKOS022188680;3-Bromo-2,6-dimethyl-4-nitropyridine1-oxide;3-Bromo-2,6-dimethyl-4-nitro-1-oxo-1lambda~5~-pyridine

Suppliers and Price of 3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide

Chemical Property:

PSA：71.28000
LogP:2.92580
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:245.96400
Heavy Atom Count:13
Complexity:208

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=[N+]1[O-])C)Br)[N+](=O)[O-]

Technology Process of 3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide

There total 1 articles about 3-Bromo-2,6-dimethyl-4-nitropyridine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3430-31-7
3-bromo-2,6-dimethylpyridine

: 54754-75-5
3‐bromo‐2,6‐dimethyl‐4‐nitropyridine 1‐oxide

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; acetic acid / 12 h / Reflux

2: nitric acid; sulfuric acid / 10 h / Reflux

With sulfuric acid; dihydrogen peroxide; nitric acid; acetic acid;
DOI:10.1002/anie.201606223

Reference yield:

: 54754-75-5
3‐bromo‐2,6‐dimethyl‐4‐nitropyridine 1‐oxide

: 33259-24-4
3-bromo-4-amino-2,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / CHCl₃ / Ambient temperature

2: 1.) PBr₃, 2.) hydrazine hydrate / 2.) Raney-Ni / 1.) CHCl₃, reflux, 1 h, 2.) CHCl₃, C₂H₅OH, reflux, 1 h

With phosphorus tribromide; hydrazine hydrate; nickel; In chloroform;

Reference yield:

: 54754-75-5
3‐bromo‐2,6‐dimethyl‐4‐nitropyridine 1‐oxide

: 76591-69-0
3,4-dibromo-2,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / CHCl₃ / Ambient temperature

2: 1.) PBr₃, 2.) hydrazine hydrate / 2.) Raney-Ni / 1.) CHCl₃, reflux, 1 h, 2.) CHCl₃, C₂H₅OH, reflux, 1 h

With phosphorus tribromide; hydrazine hydrate; nickel; In chloroform;