2-(Benzoylamino)-3,3-dichloroacrylic acid

Base Information

Chemical Name:2-(Benzoylamino)-3,3-dichloroacrylic acid
CAS No.:54902-23-7
Molecular Formula:C10H7Cl2NO3
Molecular Weight:260.076
Hs Code.:2924299090
European Community (EC) Number:688-642-3
ChEMBL ID:CHEMBL1577867

Synonyms:2-(benzoylamino)-3,3-dichloroacrylic acid;54902-23-7;MLS000573659;CHEMBRDG-BB 5142697;SMR000184507;3,3-dichloro-2-(phenylformamido)prop-2-enoic acid;2-benzamido-3,3-dichloroprop-2-enoic acid;cid_724058;SCHEMBL5041032;CHEMBL1577867;BDBM51972;HMS2374H05;STL216764;AKOS002347300;2-benzamido-3,3-dichloro-acrylic acid;2-benzamido-3,3-dichloro-2-propenoic acid;3,3-dichloro-2-(benzoylamino)acrylic acid;2-benzamido-3,3-bis(chloranyl)prop-2-enoic acid;SR-01000196797;SR-01000196797-1;3,3-dichloro-2-[(phenylcarbonyl)amino]prop-2-enoic acid

Suppliers and Price of 2-(Benzoylamino)-3,3-dichloroacrylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-BENZOYLAMINO-3,3-DICHLORO-ACRYLIC ACID Aldrich
100mg
$ 57.00

American Custom Chemicals Corporation
2-(BENZOYLAMINO)-3,3-DICHLOROACRYLIC ACID 95.00%
5MG
$ 501.34

Total 1 raw suppliers

Chemical Property of 2-(Benzoylamino)-3,3-dichloroacrylic acid

Chemical Property:

Vapor Pressure:5.29E-08mmHg at 25°C
Boiling Point:425.6oC at 760 mmHg
Flash Point:211.2oC
PSA：66.40000
Density:1.499g/cm3
LogP:2.53860
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:258.9802985
Heavy Atom Count:16
Complexity:318

Purity/Quality:

99% ^*data from raw suppliers

2-BENZOYLAMINO-3,3-DICHLORO-ACRYLIC ACID Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)NC(=C(Cl)Cl)C(=O)O

Technology Process of 2-(Benzoylamino)-3,3-dichloroacrylic acid

There total 5 articles about 2-(Benzoylamino)-3,3-dichloroacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 49837-70-9
2-benzoylamino-3,3-dichloroacrylonitrile

: 54902-23-7
3,3-dichloro-2-(benzoylamino)acrylic acid

Guidance literature:: With hydrogenchloride; water; for 0.25h; Reflux;
DOI:10.1134/S1070363221030026

Reference yield:

: 55-21-0,27208-38-4
benzamide

: 54902-23-7
3,3-dichloro-2-(benzoylamino)acrylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 2 h / 100 - 110 °C

2: thionyl chloride / benzene / 4 h / Reflux

3: water; 1,4-dioxane / 2 h / -8 - 25 °C

4: hydrogenchloride; water / 0.25 h / Reflux

With hydrogenchloride; thionyl chloride; sulfuric acid; water; In 1,4-dioxane; water; benzene;
DOI:10.1134/S1070363221030026

Reference yield:

: 6316-07-0
N-(2,2,2-trichloro-1-hydroxyethyl)benzamide

: 54902-23-7
3,3-dichloro-2-(benzoylamino)acrylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / benzene / 4 h / Reflux

2: water; 1,4-dioxane / 2 h / -8 - 25 °C

3: hydrogenchloride; water / 0.25 h / Reflux

With hydrogenchloride; thionyl chloride; water; In 1,4-dioxane; water; benzene;
DOI:10.1134/S1070363221030026