Benzene, 1,4-bis[(4-nitrophenyl)thio]-

Base Information

Chemical Name:Benzene, 1,4-bis[(4-nitrophenyl)thio]-
CAS No.:54952-19-1
Molecular Formula:C18H12N2O4S2
Molecular Weight:384.42900
Hs Code.:
DSSTox Substance ID:DTXSID30487264
Wikidata:Q82329225

Synonyms:Benzene, 1,4-bis[(4-nitrophenyl)thio]-;54952-19-1;DTXSID30487264;1,4-bis(4'-nitrophenylthio)benzene

Suppliers and Price of Benzene, 1,4-bis[(4-nitrophenyl)thio]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of Benzene, 1,4-bis[(4-nitrophenyl)thio]-

Chemical Property:

Melting Point:218 °C
Boiling Point:609.8±50.0 °C(Predicted)
PSA：142.24000
Density:1.47±0.1 g/cm3(Predicted)
LogP:6.85180
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:384.02384922
Heavy Atom Count:26
Complexity:429

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])SC2=CC=C(C=C2)SC3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of Benzene, 1,4-bis[(4-nitrophenyl)thio]-

There total 5 articles about Benzene, 1,4-bis[(4-nitrophenyl)thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 136286-78-7
copper(I) 4-nitrophenylthiolate

: 106-37-6
1.4-dibromobenzene

: 54952-19-1
1,4-bis(4-nitrophenylsulfenyl)benzene

Guidance literature:: In pyridine; quinoline; at 200 ℃; for 2h;
DOI:10.1002/ejoc.200901042

Reference yield:

: 624-39-5
benzene-1,4-dithiol

: 100-00-5
4-chlorobenzonitrile

: 54952-19-1
1,4-bis(4-nitrophenylsulfenyl)benzene

Guidance literature:: With sodium hydroxide;

Reference yield:

: 101-59-7
4-amino-4'-nitrodiphenyl sulfide

: 54952-19-1
1,4-bis(4-nitrophenylsulfenyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. NaNO₂, 7percent HCl, 2.) aq. KI / 1.) 0 deg C, 1 h, 2.) 60 deg C, 2 h

2: 2.) copper / 1.) methanol, reflux, 15 min, 2.) DMF, 140 deg C, 2 h

With hydrogenchloride; copper; potassium iodide; sodium nitrite;
DOI:10.1007/BF00960284