N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1)

Base Information

Chemical Name:N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1)
CAS No.:112764-13-3
Molecular Formula:C₂₁H₂₂N₂O₃*ClH
Molecular Weight:386.878
Hs Code.:

Synonyms:Propanamide,3-(diethylamino)-N-(9,10-dihydro-9,10-dioxo-1-anthracenyl)-, monohydrochloride(9CI)

Suppliers and Price of N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1)

Chemical Property:

Vapor Pressure:3.12E-13mmHg at 25°C
Boiling Point:575.2°Cat760mmHg
Flash Point:301.7°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1)

There total 2 articles about N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-N~3~,N~3~-diethyl-beta-alaninamide hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 20210-30-4
N-(9,10-dihydro-9,10-dioxo-1-anthracenyl)-3-chloropropanamide

: 109-89-7
diethylamine

: 112764-13-3
3-(diethylamino)-N-(9,10-dihydro-9,10-dioxoanthracen-1-yl)propanamide hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 70 ℃; for 7h;
DOI:10.1021/jm00399a028

Reference yield:

: 82-45-1
1-amino-9,10-anthracenedione

: 112764-13-3
3-(diethylamino)-N-(9,10-dihydro-9,10-dioxoanthracen-1-yl)propanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / pyridine / toluene / 5 h / 60 °C

2: 77 percent / 2.) aq. HCl / ethanol / 7 h / 70 °C

With pyridine; hydrogenchloride; In ethanol; toluene;
DOI:10.1021/jm00399a028