Cyclobutanone, 3-(phenylmethyl)-

Base Information

Chemical Name:Cyclobutanone, 3-(phenylmethyl)-
CAS No.:55262-02-7
Molecular Formula:C11H12O
Molecular Weight:160.216
Hs Code.:

Synonyms:

Suppliers and Price of Cyclobutanone, 3-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Benzylcyclobutanone
10mg
$ 45.00

Labseeker
3-benzylcyclobutanone 95
2g
$ 1083.00

Crysdot
3-Benzylcyclobutanone 95+%
1g
$ 386.00

AK Scientific
3-Benzylcyclobutanone
1g
$ 1091.00

AK Scientific
3-Benzylcyclobutanone
250mg
$ 464.00

Total 4 raw suppliers

Chemical Property of Cyclobutanone, 3-(phenylmethyl)-

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

99% ^*data from raw suppliers

3-Benzylcyclobutanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclobutanone, 3-(phenylmethyl)-

There total 5 articles about Cyclobutanone, 3-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 201230-82-2
carbon monoxide

: 106-95-6
allyl bromide

: 620-05-3
iodomethylbenzene

: 55262-02-7
3-benzyl-cyclobutanone

Guidance literature:: allyl bromide; With [(η5-pentamethylcyclopentadienyl)2TiCl]; In tetrahydrofuran; at -35 ℃; for 0.0166667h;

iodomethylbenzene; With samarium diiodide; In tetrahydrofuran; at -35 - 20 ℃;

carbon monoxide; In pentane; at 45 ℃; for 12h; under 517.162 Torr; Further stages.;
DOI:10.1021/ja0158657

Reference yield: 78.0%

: 55262-01-6
1-methylsulfinyl-1-methylthio-3-benzylcyclobutane

: 55262-02-7
3-benzyl-cyclobutanone

Guidance literature:: With sulfuric acid; In diethyl ether; 1.) room temperature, 1d, 2.) reflux, 7h;
DOI:10.1246/bcsj.57.1637

Reference yield:

: 300-57-2,57807-91-7
allylbenzene

: 55262-02-7
3-benzyl-cyclobutanone

Guidance literature:: Multi-step reaction with 2 steps

1: zinc/copper couple; trichlorophosphate / diethyl ether / Reflux

2: acetic acid; zinc / 7 h / 20 - 80 °C

With zinc/copper couple; acetic acid; zinc; trichlorophosphate; In diethyl ether;
DOI:10.1016/j.tet.2012.03.108