Benzenepropanol, b-bromo-, acetate

Base Information

Chemical Name:Benzenepropanol, b-bromo-, acetate
CAS No.:55510-09-3
Molecular Formula:C₁₁H₁₃BrO₂
Molecular Weight:257.127
Hs Code.:

Synonyms:

Suppliers and Price of Benzenepropanol, b-bromo-, acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanol, b-bromo-, acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanol, b-bromo-, acetate

There total 3 articles about Benzenepropanol, b-bromo-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 300-57-2,57807-91-7
allylbenzene

: 64-19-7,77671-22-8
acetic acid

: 55510-09-3
1-acetoxy-2-bromo-3-phenylpropane

: 55510-08-2
1-bromo-3-phenylpropan-2-yl acetate

Guidance literature:: With bromine; lithium perchlorate; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja00009a032

Reference yield:

: 300-57-2,57807-91-7
allylbenzene

: 55510-09-3
1-acetoxy-2-bromo-3-phenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / t-C₄H₉-OOH, aq. 40percent Triton B, OsO₄ / 2-methyl-propan-2-ol / 0 °C

2: 2-acetoxybenzoyl bromide / 2 h / 100 °C

With tert.-butylhydroperoxide; osmium(VIII) oxide; N-benzyl-trimethylammonium hydroxide; 2-Acetoxybenzoyl bromide; In tert-butyl alcohol;
DOI:10.1055/s-1984-30758

Reference yield:

: 1821-12-1
4-Phenylbutyric acid

: 55510-09-3
1-acetoxy-2-bromo-3-phenylpropane

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / Pb(OAc)4, Cu(OAc)2, pyridine / benzene / 8 h / Heating

2: 80 percent / t-C₄H₉-OOH, aq. 40percent Triton B, OsO₄ / 2-methyl-propan-2-ol / 0 °C

3: 2-acetoxybenzoyl bromide / 2 h / 100 °C

With pyridine; lead(IV) acetate; tert.-butylhydroperoxide; osmium(VIII) oxide; copper diacetate; N-benzyl-trimethylammonium hydroxide; 2-Acetoxybenzoyl bromide; In tert-butyl alcohol; benzene;
DOI:10.1055/s-1984-30758