2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)-

Base Information

Chemical Name:2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)-
CAS No.:55739-56-5
Molecular Formula:C14H15NO6
Molecular Weight:293.276
Hs Code.:

Synonyms:3-methoxy-4-acetoxy-(Z)-α-acetamidocinnamic acid;(Z)-α-Acetamido-4-acetoxy-3-methoxycinnamic Acid;α-acetamido-3-methoxy-4-acetoxycinnamic acid;p-acetoxy-m-methoxy α-acetamido cinnamic acid;4-Acetoxy-α-acetylamino-3-methoxyzimtsaeure;β-(3-methoxy-4-acetoxyphenyl)-α-acetamidoacrylic acid;

Suppliers and Price of 2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)-

Chemical Property:

PSA：101.93000
LogP:1.57300

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)-

There total 4 articles about 2-Propenoic acid, 2-(acetylamino)-3-[4-(acetyloxy)-3-methoxyphenyl]-, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 60470-82-8
(Z)-2-methoxy-4-((2-methyl-5-oxooxazol-4(5H)-ylidene)methyl)phenyl acetate

: 55739-56-5
α-acetamido-3-methoxy-4-acetoxycinnamic acid

Guidance literature:: With water; sodium acetate; In acetone; at 80 ℃; for 1.5h;
DOI:10.1055/s-1992-26228

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 55739-56-5
α-acetamido-3-methoxy-4-acetoxycinnamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaOAc / 4 h / 120 °C

2: 92 percent / NaOAc, H₂O / acetone / 1.5 h / 80 °C

With water; sodium acetate; In acetone;
DOI:10.1055/s-1992-26228