2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)-

Base Information

Chemical Name:2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)-
CAS No.:55882-65-0
Molecular Formula:C₁₂H₁₁ClO₄
Molecular Weight:254.67
Hs Code.:

Synonyms:4-O-acetylferulic acid chloride;4-acetoxy-3-methoxycinnamoyl chloride;acetic acid 4-(2-chlorocarbonyl-vinyl)-2-methoxyphenyl ester;3-methoxy-4-acetyloxycinnamoyl chloride;4-Oacetylferulic acid chloride;3-(4-acetoxy-3-methoxyphenyl)acryloyl chloride;

Suppliers and Price of 2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(2E)-3-[4-(Acetyloxy)-3-methoxyphenyl]-2-propenoylChloride
100mg
$ 925.00

TRC
(2E)-3-[4-(Acetyloxy)-3-methoxyphenyl]-2-propenoylChloride
25mg
$ 305.00

TRC
(2E)-3-[4-(Acetyloxy)-3-methoxyphenyl]-2-propenoylChloride
10mg
$ 130.00

Total 0 raw suppliers

Chemical Property of 2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)-

Chemical Property:

Boiling Point:352.3±27.0 °C(Predicted)
PSA：52.60000
Density:1.269±0.06 g/cm3(Predicted)
LogP:2.39910

Purity/Quality:: (2E)-3-[4-(Acetyloxy)-3-methoxyphenyl]-2-propenoylChloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses (2E)-3-[4-(Acetyloxy)-3-methoxyphenyl]-2-propenoyl Chloride is used in the synthesis of target compound of Feruloyl Arabinofuranoside; Also, it is an intermediate used in the synthesis of 3-O-(E)-Feruloylquinic Acid (F308980), which is a phenolic acid with potential antioxidant and antifungal activities. Secondary metabolite in the coffee brewing process.

Technology Process of 2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)-

There total 5 articles about 2-Propenoyl chloride, 3-[4-(acetyloxy)-3-methoxyphenyl]-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 34749-55-8,147677-05-2,2596-47-6
3-(4-acetoxy-3-methoxyphenyl)prop-2-enoic acid

: 55882-65-0,108608-07-7,50906-12-2
4-acetoxyferuloyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In chloroform; for 4h; Reflux;
DOI:10.1007/s11172-014-0710-8

Reference yield:

: 1135-24-6,537-98-4
3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 55882-65-0,108608-07-7,50906-12-2
4-acetoxyferuloyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / pyridine / 2 h / 0 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 0 - 20 °C

With dmap; oxalyl dichloride; N,N-dimethyl-formamide; In pyridine; toluene;
DOI:10.1002/rcm.4537

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 55882-65-0,108608-07-7,50906-12-2
4-acetoxyferuloyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate

2: thionyl chloride

With thionyl chloride; sodium acetate;