(1-Chloro-3-methoxypropyl)benzene

Base Information

• Chemical Name: (1-Chloro-3-methoxypropyl)benzene
• CAS No.: 55955-55-0
• Molecular Formula: C10H13ClO
• Molecular Weight: 184.666
• Mol file: 55955-55-0.mol

Synonyms:3-Chlor-3-phenyl-propyl-methylether;3-chloro-1-methoxy-3-phenylpropane;methyl 3-chloro-3-phenylpropyl ether;3-Methoxy-1-phenylpropylchlorid;

Chemical Property of (1-Chloro-3-methoxypropyl)benzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.00300

Purity/Quality:

99% ^*data from raw suppliers

(1-Chloro-3-methoxypropyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1-Chloro-3-methoxypropyl)benzene

There total 5 articles about (1-Chloro-3-methoxypropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + chloromethyl methyl ether (107-30-2) → methyl 3-chloro-3-phenylpropyl ether (55955-55-0)

Guidance literature:

With tin(IV) chloride; at 45 - 60 ℃; for 0.166667h;

DOI:10.1134/S0965544107020089

Reference yield: 90.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Dimethoxymethane (109-87-5) → methyl 3-chloro-3-phenylpropyl ether (55955-55-0)

Guidance literature:

Dimethoxymethane; With chlorosulfonic acid; zinc(II) chloride; at -10 ℃; for 0.5h;

styrene; at 5 - 10 ℃; for 2h;

DOI:10.1080/00397911.2019.1571209

Reference yield: 75.0%

chloromethyl methyl ether (107-30-2) + (1-chloroethyl)benzene (672-65-1) → methyl 3-chloro-3-phenylpropyl ether (55955-55-0)

Guidance literature:

With zinc(II) chloride; In hexane; at 60 ℃; for 4h;

DOI:10.14233/ajchem.2018.20876

upstream raw materials:

styrene

methanol

formaldehyd

Dimethoxymethane

Downstream raw materials:

5-Methoxy-3-phenyl-pentan-1-ol

(1,4-dimethoxybutan-2-yl)benzene

1-Phenyl-1-(β-hydroxy-aethylamino)-3-methoxy-propan

1-Phenyl-1--3-methoxy-propan