1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione

Base Information

• Chemical Name: 1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione
• CAS No.: 56043-02-8
• Molecular Formula: C₁₄H₉NS₃
• Molecular Weight: 287.43
• DSSTox Substance ID: DTXSID20518410
• Wikidata: Q82381088
• Mol file: 56043-02-8.mol

Synonyms:56043-02-8;1-phenyl-1H-benzo[d][1,3]thiazine-2,4-dithione;1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione;DTXSID20518410

Chemical Property of 1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 286.98971281
• Heavy Atom Count: 18
• Complexity: 349

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N2C3=CC=CC=C3C(=S)SC2=S

Technology Process of 1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione

There total 1 articles about 1-Phenyl-2H-3,1-benzothiazine-2,4(1H)-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenyl isatoic anhydride (20877-86-5) → N-Phenyl-trithioisatosaeureanhydrid (56043-02-8)

Guidance literature:

With tetraphosphorus decasulfide; In pyridine;

Reference yield: 85.0%

N-Phenyl-trithioisatosaeureanhydrid (56043-02-8) + anthranilic acid hydrazide (1904-58-1) → C20H16N4S

Guidance literature:

In various solvent(s); for 2h;

DOI:10.1007/BF00799952

Reference yield: 64.0%

N-Phenyl-trithioisatosaeureanhydrid (56043-02-8) + isoniazid (54-85-3,7640-37-1) → Phenyl-[2-(5-pyridin-4-yl-[1,3,4]thiadiazol-2-yl)-phenyl]-amine

Guidance literature:

In various solvent(s); for 2h;

DOI:10.1007/BF00799952

upstream raw materials:

N-phenyl isatoic anhydride

Downstream raw materials:

[2-(morpholine-4-carbothioyl)-phenyl]-phenyl-dithiocarbamic acid

pyrazolidine‐3,5‐dione

2,5-Bis(2-phenylamino-phenyl)-1,3,4-thiadiazol

N-(4-Chloro-phenyl)-2-phenylamino-thiobenzamide