Technology Process of 2,4-Imidazolidinedione, 3-(2-methylphenyl)-5-(phenylmethyl)-
There total 3 articles about 2,4-Imidazolidinedione, 3-(2-methylphenyl)-5-(phenylmethyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(2-Methylphenyl)-hydantoin;
With
methyl magnesium carbonate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 1.5h;
benzyl bromide;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 5h;
DOI:10.1246/bcsj.74.1917
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 73 percent / KOH / H2O / 20 °C
2.1: 92 percent / HCl / H2O / 2 h / Heating
3.1: magnesium methyl carbonate / dimethylformamide / 1.5 h / 80 °C
3.2: 64 percent / dimethylformamide / 5 h / 110 °C
With
hydrogenchloride; potassium hydroxide; methyl magnesium carbonate;
In
water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.74.1917
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 92 percent / HCl / H2O / 2 h / Heating
2.1: magnesium methyl carbonate / dimethylformamide / 1.5 h / 80 °C
2.2: 64 percent / dimethylformamide / 5 h / 110 °C
With
hydrogenchloride; methyl magnesium carbonate;
In
water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.74.1917