2,6-Dichloro-3-hydroxybenzaldehyde

Base Information

Chemical Name:2,6-Dichloro-3-hydroxybenzaldehyde
CAS No.:56962-14-2
Molecular Formula:C7H4Cl2O2
Molecular Weight:191.014
Hs Code.:
DSSTox Substance ID:DTXSID70439944
Wikidata:Q82256055

Synonyms:2,6-dichloro-3-hydroxybenzaldehyde;56962-14-2;Benzaldehyde, 2,6-dichloro-3-hydroxy-;2,6-dichloro-3-hydroxy-benzaldehyde;MFCD24673790;starbld0018248;SCHEMBL1413983;DTXSID70439944;JDTZZOXWEJEADB-UHFFFAOYSA-N;AMY17525;BS-51035;SY268236;CS-0188370;EN300-1086816;Z3244840495

Suppliers and Price of 2,6-Dichloro-3-hydroxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2,6-Dichloro-3-hydroxybenzaldehyde

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:189.9588348
Heavy Atom Count:11
Complexity:151

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1O)Cl)C=O)Cl

Technology Process of 2,6-Dichloro-3-hydroxybenzaldehyde

There total 9 articles about 2,6-Dichloro-3-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 100-83-4
meta-hydroxybenzaldehyde

: 56962-14-2
2,6-dichloro-3-hydroxybenzaldehyde

Guidance literature:: With chlorine; In acetic acid; for 4h;
DOI:10.1016/0223-5234(93)90003-W

Reference yield: 72.6%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 169619-83-4
tert-butyl-(2,4-dichloro-phenoxy)-dimethyl-silane

: 56962-14-2
2,6-dichloro-3-hydroxybenzaldehyde

Guidance literature:: tert-butyl-(2,4-dichloro-phenoxy)-dimethyl-silane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; for 1h;

With hydrogenchloride; water; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 45.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: C₁₃H₁₈Cl₂O₂Si

: 56962-14-2
2,6-dichloro-3-hydroxybenzaldehyde

Guidance literature:: tert-butyl-(2,4-dichloro-phenoxy)-dimethyl-silane; With sec.-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

N,N-dimethyl-formamide; In tetrahydrofuran; at -78 ℃; for 1.5h;

With water; acetic acid; In tetrahydrofuran; at -78 - 20 ℃;