TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE
• CAS No.: 569667-93-2
• Molecular Formula: C12H22N2O4
• Molecular Weight: 258.318
• Mol file: 569667-93-2.mol

Synonyms:tert-butyl 3-(N-methoxy-N-methylcarbamoyl)pyrrolidine-1-carboxylate;(+/-)-3-(methoxy-methyl-carbamoyl)-pyrrolidine-1-carboxylic acid tert-butyl ester;tert-butyl 3-{[(methoxy)(methyl)amino]carbonyl}pyrrolidine-1-carboxylate;tert-butyl 3-{[methoxy(methyl)amino]carbonyl}pyrrolidine-1-carboxylate;(RS)-N-Boc-3-(N-methyl-N-methoxycarbamoyl)pyrrolidine;

Chemical Property of TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE

Chemical Property:

• PSA: 59.08000
• LogP: 1.20110

Purity/Quality:

97% ^*data from raw suppliers

tert-butyl3-(methoxy(methyl)carbamoyl)pyrrolidine-1-carboxylate 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE

There total 4 articles about TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-boc-pyrrolidine-3-carboxylic acid (72925-16-7,72983-31-4,140148-70-5,59378-75-5) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → tert-butyl 3-(methoxy(methyl)carbamoyl)pyrrolidine-1-carboxylate (569667-93-2)

Guidance literature:

1-boc-pyrrolidine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 1h;

N,O-dimethylhydroxylamine*hydrochloride; In dichloromethane; at 20 ℃; for 16h; Concentration; Temperature;

Reference yield: 96.0%

N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → tert-butyl 3-(methoxy(methyl)carbamoyl)pyrrolidine-1-carboxylate (569667-93-2)

Guidance literature:

1-boc-pyrrolidine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 18 - 25 ℃; for 2h;

N,O-dimethylhydroxylamine*hydrochloride; In dichloromethane; at 18 - 25 ℃; for 18h;

Reference yield: 80.0%

→ tert-butyl 3-(methoxy(methyl)carbamoyl)pyrrolidine-1-carboxylate (569667-93-2)

Guidance literature:

With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃;

In dichloromethane; at 20 ℃;

upstream raw materials:

N,O-dimethylhydroxylamine*hydrochloride

1-boc-pyrrolidine-3-carboxylic acid

N-tert-butoxycarbonyl-proline

Downstream raw materials:

tert-butyl 3-acetylpyrrolidine-1-carboxylate

tert-butyl 3-formylpyrrolidine-1-carboxylate

1,1-dimethylethyl 3-benzoyl-1-pyrrolidinecarboxylate

(+/-)-3-(4-bromo-benzoyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 569667-93-2 TERT-BUTYL 3-(METHOXY(METHYL)CARBAMOYL)PYRROLIDINE-1-CARBOXYLATE

Send

Send

Metric Ton KG G Pound L ML

Send

Send