9-(4-(tert-butyl)phenyl)-9H-carbazole

Base Information

• Chemical Name: 9-(4-(tert-butyl)phenyl)-9H-carbazole
• CAS No.: 57103-13-6
• Molecular Formula: C22H21N
• Molecular Weight: 299.415

Synonyms:9-(4-tert-butylphenyl)-9H-carbazole;9-[4-(tert-butyl)phenyl]-9H-carbazole;9-(4-tert-Butyl-phenyl)-9H-carbazole;N-(4-tert-butylphenyl)carbazole;9-(4-tert-Butylphenyl)carbazole;9-(4-t-butylphenyl)-9H-carbazole;

Chemical Property of 9-(4-(tert-butyl)phenyl)-9H-carbazole

Chemical Property:

• Melting Point: 182 - 184 °C (ethanol)
• PSA: 4.93000
• LogP: 6.08120
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

9-[4-(tert-Butyl)phenyl]-9H-carbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(4-(tert-butyl)phenyl)-9H-carbazole

There total 14 articles about 9-(4-(tert-butyl)phenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.21%

4-tert-Butylaniline (769-92-6) + [1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate (189999-35-7) → 9-(4-(tert-butyl)phenyl)-9H-carbazole (57103-13-6)

Guidance literature:

With copper diacetate; sodium carbonate; In ethylene glycol; isopropyl alcohol; at 90 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.ejmech.2013.07.029

Reference yield: 98.0%

4-tert-butylphenyl mesylate (59970-38-6) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 9-(4-(tert-butyl)phenyl)-9H-carbazole (57103-13-6)

Guidance literature:

With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; potassium carbonate; phenylboronic acid; In tert-butyl alcohol; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.200802157

Reference yield: 96.0%

4-tert-butylphenyltosylate (7598-28-9) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 9-(4-(tert-butyl)phenyl)-9H-carbazole (57103-13-6)

Guidance literature:

With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; potassium carbonate; phenylboronic acid; In tert-butyl alcohol; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1002/asia.201800575

upstream raw materials:

1-bromo-4-tert-butylbenzene

9H-carbazole

4-tert-butylphenyl mesylate

1-tert-butyl-4-iodobenzene

Downstream raw materials:

C₆₀H₄₃Br₂N

C₆₀H₄₃Br₂N

9-(4-tert-butylphenyl)-3-bromo-9H-carbazole

9-(4-tert-butylphenyl)-3-(thiophen-2-yl)-9H-carbazole

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