Technology Process of Silane, trimethyl[(1E)-1-methyl-2-phenylethenyl]-
There total 13 articles about Silane, trimethyl[(1E)-1-methyl-2-phenylethenyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
In
tetrahydrofuran;
for 120h;
Ambient temperature;
DOI:10.1039/P19960002803
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / HCl, H2S / diethyl ether / -30 °C
2: 98 percent / K2CO3 / acetone / Ambient temperature
3: 94 percent / Ni(dppe)Cl2 / tetrahydrofuran / 120 h / Ambient temperature
With
hydrogenchloride; hydrogen sulfide; potassium carbonate;
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
In
tetrahydrofuran; diethyl ether; acetone;
DOI:10.1039/P19960002803
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / K2CO3 / acetone / Ambient temperature
2: 94 percent / Ni(dppe)Cl2 / tetrahydrofuran / 120 h / Ambient temperature
With
potassium carbonate;
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
In
tetrahydrofuran; acetone;
DOI:10.1039/P19960002803