Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate

Base Information

Chemical Name:Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate
CAS No.:57337-92-5
Molecular Formula:C₁₄H₁₄ClNO₆
Molecular Weight:327.721
Hs Code.:
DSSTox Substance ID:DTXSID60488608

Synonyms:57337-92-5;Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate;DTXSID60488608

Suppliers and Price of Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:327.0509649
Heavy Atom Count:22
Complexity:442

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=C(C1=CC=C(C=C1)[N+](=O)[O-])Cl)C(=O)OCC

Technology Process of Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate

There total 4 articles about Diethyl [chloro(4-nitrophenyl)methylidene]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₂BrNO₅S

: 57337-92-5
2-[Chloro-(4-nitro-phenyl)-methylene]-malonic acid diethyl ester

Guidance literature:: With lithium chloride; In tert-butyl alcohol;
DOI:10.1039/P29750000863

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 57337-92-5
2-[Chloro-(4-nitro-phenyl)-methylene]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; magnesium chloride / acetonitrile / 0 - 20 °C

2: tributyl-amine; trichlorophosphate / Reflux

With tributyl-amine; triethylamine; magnesium chloride; trichlorophosphate; In acetonitrile;
DOI:10.3762/bjoc.7.95

Reference yield:

: 105-53-3
diethyl malonate

: 57337-92-5
2-[Chloro-(4-nitro-phenyl)-methylene]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; magnesium chloride / acetonitrile / 0 - 20 °C

2: tributyl-amine; trichlorophosphate / Reflux

With tributyl-amine; triethylamine; magnesium chloride; trichlorophosphate; In acetonitrile;
DOI:10.3762/bjoc.7.95