2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-

Base Information

Chemical Name:2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-
CAS No.:58112-92-8
Molecular Formula:C16H14N2S
Molecular Weight:266.367
Hs Code.:
DSSTox Substance ID:DTXSID10482434

Synonyms:58112-92-8;2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-;DTXSID10482434

Suppliers and Price of 2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:266.08776963
Heavy Atom Count:19
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=S)CC(=NC2=CC=CC=C21)C3=CC=CC=C3

Technology Process of 2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl-

There total 3 articles about 2H-1,5-Benzodiazepine-2-thione, 1,3-dihydro-1-methyl-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 58876-61-2
1-methyl-4-phenyl-1H-benzo[b][1,4]diazepin-2(3H)-one

: 58112-92-8
methyl-1 phenyl-4 benzodiazepine-1,5 thione-2

Guidance literature:: With tetraphosphorus decasulfide; In pyridine; at 100 - 110 ℃; for 1h; Heating;
DOI:10.1007/BF00472558

Reference yield:

: 16439-95-5
4-phenyl-2,3-dihydro-1H-1,5-benzodiazepin-2-one

: 58112-92-8
methyl-1 phenyl-4 benzodiazepine-1,5 thione-2

Guidance literature:: Multi-step reaction with 2 steps

2: 89 percent / P₂S₅ / pyridine / 1 h / 100 - 110 °C / Heating

With tetraphosphorus decasulfide; In pyridine;
DOI:10.1007/BF00472558