N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide

Base Information

Chemical Name:N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide
CAS No.:58131-63-8
Molecular Formula:C22H22NOP
Molecular Weight:347.397
Hs Code.:
DSSTox Substance ID:DTXSID00453214
Nikkaji Number:J1.152.083I
Wikidata:Q82274304

Synonyms:58131-63-8;N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide;SCHEMBL9203590;Acetamide, N,N-dimethyl-2-(triphenylphosphoranylidene)-;DTXSID00453214

Suppliers and Price of N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:347.143901323
Heavy Atom Count:25
Complexity:428

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C(=O)C=P(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide

There total 4 articles about N,N-Dimethyl-2-(triphenylphosphoranylidene)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 603-35-0
triphenylphosphine

: 2675-89-0
2-chloro-N,N-dimethylacetamide

: 58131-63-8
<(N,N-dimethylcarbamoyl)methylene>triphenylphosphorane

Guidance literature:: In diethyl ether; for 26h; Reflux;
DOI:10.1021/jacs.0c11462

Reference yield: 76.0%

: 113204-09-4
[(dimethylcarbamoyl)methyl]triphenylphosphonium chloride

: 58131-63-8
<(N,N-dimethylcarbamoyl)methylene>triphenylphosphorane

Guidance literature:: With sodium hydride; In dichloromethane; for 0.5h;
DOI:10.1039/DT9910002579

Reference yield:

: 603-35-0
triphenylphosphine

: 58131-63-8
<(N,N-dimethylcarbamoyl)methylene>triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / diethyl ether / 2 h / Heating

2: 65 percent / 5percent NaOH / H₂O; CH₂Cl₂ / 2 h

With sodium hydroxide; In diethyl ether; dichloromethane; water;