3-Oxazolidinecarboxylic acid, 4-(3-chloro-3-oxopropyl)-5-oxo-, phenylmethyl ester, (S)-

Base Information

Chemical Name:3-Oxazolidinecarboxylic acid, 4-(3-chloro-3-oxopropyl)-5-oxo-, phenylmethyl ester, (S)-
CAS No.:58456-26-1
Molecular Formula:C14H14ClNO5
Molecular Weight:311.722
Hs Code.:

Synonyms:(S)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinepropionyl chloride;(4S)-3-(benzyloxycarbonyl)-4-(3-chloro-3-oxopropyl)-1,3-oxazolidin-5-one;(4S)-4-[2-(Chloroformyl)ethyl]-3-[(phenylmethoxy)carbonyl]oxazolidin-5-one;3-[(4S)-3-benzyloxycarbonyl-5-oxo-1,3-oxazolidin-4-yl]propionyl chloride;(S)-3-[3-(benzyloxycarbonyl)-5-oxooxazolidin-4-yl]-propanoyl chloride;(S)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinepropanoyl chloride;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Oxazolidinecarboxylic acid, 4-(3-chloro-3-oxopropyl)-5-oxo-, phenylmethyl ester, (S)-

Chemical Property:

PSA：72.91000
LogP:1.99160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Oxazolidinecarboxylic acid, 4-(3-chloro-3-oxopropyl)-5-oxo-, phenylmethyl ester, (S)-

There total 5 articles about 3-Oxazolidinecarboxylic acid, 4-(3-chloro-3-oxopropyl)-5-oxo-, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 23632-67-9
(S)-3-[3-(benzyloxycarbonyl)-5-oxooxazolidin-4-yl]propanoic acid

: 58456-26-1
(S)-4-<2'-(Chloroformyl)ethyl>-5-oxooxazolidin-3-carbonsaeure-benzylester

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo026479q

Reference yield:

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 58456-26-1
(S)-4-<2'-(Chloroformyl)ethyl>-5-oxooxazolidin-3-carbonsaeure-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: CSA / toluene / Heating

2: SOCl₂ / 0.25 h / Heating

With thionyl chloride; camphor-10-sulfonic acid; In toluene;
DOI:10.1002/hlca.200690235

Reference yield:

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 58456-26-1
(S)-4-<2'-(Chloroformyl)ethyl>-5-oxooxazolidin-3-carbonsaeure-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-toluenesulfonic acid / toluene / 1.67 h / Heating

2: 100 percent / oxalyl chloride; DMF / CH₂Cl₂ / 0.5 h / 20 °C

With oxalyl dichloride; toluene-4-sulfonic acid; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1021/jo026479q