Azoxybenzene-3,3'-dicarboxylic acid

Base Information

• Chemical Name: Azoxybenzene-3,3'-dicarboxylic acid
• CAS No.: 587-55-3
• Molecular Formula: C14H10N2O5
• Molecular Weight: 286.244
• Mol file: 587-55-3.mol

Synonyms:Benzoic acid, 3,3‘-azoxybis-;

Chemical Property of Azoxybenzene-3,3'-dicarboxylic acid

Chemical Property:

• Melting Point: 310-320 °C
• Boiling Point: 597.7±60.0 °C(Predicted)
• PSA: 115.71000
• Density: 1.41±0.1 g/cm3(Predicted)
• LogP: 3.53190

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Azoxybenzene-3,3'-dicarboxylic acid

There total 23 articles about Azoxybenzene-3,3'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

meta-aminobenzoic acid (99-05-8,159139-79-4) → 3,3'-azoxybis-benzoic acid (587-55-3)

Guidance literature:

With sodium tungstate; phosphoric acid; dihydrogen peroxide; In ethanol; at 60 - 65 ℃;

Reference yield:

3-nitro-benzaldehyde (99-61-6) → 3,3'-azoxybis-benzoic acid (587-55-3) + 3-nitrobenzoic acid (121-92-6)

Guidance literature:

With sodium hydroxide;

Reference yield:

1-methyl-4-nitrosobenzene (623-11-0) + 3-nitro-benzaldehyde (99-61-6) → 3,3'-azoxybis-benzoic acid (587-55-3) + 3-nitrobenzoic acid (121-92-6)

Guidance literature:

at 80 - 100 ℃;

upstream raw materials:

m-azoxybenzaldehyde

1-methyl-4-nitrosobenzene

3-nitro-benzaldehyde

D-glucose

Downstream raw materials:

4,4'-diamino-[1,1'-biphenyl]-2,2'-dicarboxylic acid

3,3'-azodibenzoic acid