1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene

Base Information

Chemical Name:1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene
CAS No.:58811-50-0
Molecular Formula:C9H6BrNO3
Molecular Weight:256.056
Hs Code.:
DSSTox Substance ID:DTXSID50544444
Wikidata:Q82421544

Synonyms:58811-50-0;1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene;DTXSID50544444

Suppliers and Price of 1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:254.95311
Heavy Atom Count:14
Complexity:254

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])OCC#CBr

Technology Process of 1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene

There total 3 articles about 1-[(3-Bromoprop-2-yn-1-yl)oxy]-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 58811-50-0
3-bromo-2-propynyl-4-nitrophenyl ether

Guidance literature:: With potassium hydroxide; bromine; In 1,4-dioxane; water; for 1h; Ambient temperature;
DOI:10.1002/bbpc.19870910920

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 58811-50-0
3-bromo-2-propynyl-4-nitrophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / K₂CO₃ / acetone / 20 h / Heating

2: 97 percent / KOH, Br₂ / H₂O; dioxane / 1 h / Ambient temperature

With potassium hydroxide; bromine; potassium carbonate; In 1,4-dioxane; water; acetone;
DOI:10.1002/bbpc.19870910920