5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine

Base Information

Chemical Name:5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine
CAS No.:58943-96-7
Molecular Formula:C19H16NOP
Molecular Weight:305.316
Hs Code.:
DSSTox Substance ID:DTXSID90502220
Wikidata:Q82355072

Synonyms:58943-96-7;5-methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine;SCHEMBL19660984;DTXSID90502220;5-Methyl-10-phenyl-5,10-dihydro-10lambda~5~-phenazaphosphinin-10-one

Suppliers and Price of 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:305.096951132
Heavy Atom Count:22
Complexity:417

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2P(=O)(C3=CC=CC=C31)C4=CC=CC=C4

Technology Process of 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine

There total 15 articles about 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (2-(methyl(phenyl)amino)phenyl)(phenyl)phosphine oxide

: 58943-96-7
5-methyl-10-phenyl-5,10-dihydrophenophosphazinine 10-oxide

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; tetrabutylammonium tetrafluoroborate; In water; acetonitrile; at 25 ℃; for 10.73h; Inert atmosphere; Electrochemical reaction;
DOI:10.1021/acs.orglett.1c00807

Reference yield:

: 896-84-4
5-methyl-10-phenyl-5,10-dihydrophenophosphazinine

: 58943-96-7
5-methyl-10-phenyl-5,10-dihydrophenophosphazinine 10-oxide

Guidance literature:: With tris-(trimethylsilyl)silane; palladium diacetate; In N,N-dimethyl-formamide; at 130 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1021/ol503252t

Reference yield:

: 58476-60-1
(2'-bromophenyl)-(2-nitrophenyl)-amine

: 58943-96-7
5-methyl-10-phenyl-5,10-dihydrophenophosphazinine 10-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: dimethyl sulfoxide / 3 h / Inert atmosphere; Sealed tube

2: iron; ammonium chloride / ethanol; water / 3 h / Sealed tube; Reflux

3: sodium nitrite; potassium iodide; toluene-4-sulfonic acid / water; acetonitrile / 0 - 20 °C / Sealed tube

4: copper(l) iodide; caesium carbonate / toluene / 48 h / 110 °C / Sealed tube; Inert atmosphere

5: tris-(trimethylsilyl)silane; palladium diacetate / N,N-dimethyl-formamide / 12 h / 130 °C / Inert atmosphere; Sealed tube

6: tris-(trimethylsilyl)silane; palladium diacetate / N,N-dimethyl-formamide / 12 h / 130 °C / Inert atmosphere; Sealed tube

With copper(l) iodide; tris-(trimethylsilyl)silane; palladium diacetate; iron; ammonium chloride; caesium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol503252t