Ethyl 3-methylpyridine-2-carboxylate

Base Information

Chemical Name:Ethyl 3-methylpyridine-2-carboxylate
CAS No.:58997-10-7
Molecular Formula:C₉H₁₁NO₂
Molecular Weight:165.192
Hs Code.:2933399090
DSSTox Substance ID:DTXSID70482096
Wikidata:Q72476179
Mol file:58997-10-7.mol

Synonyms:58997-10-7;ETHYL 3-METHYLPYRIDINE-2-CARBOXYLATE;ethyl 3-methylpicolinate;MFCD11616893;ETHYL 3-METHYL-2-PYRIDINECARBOXYLATE;Ethyl3-Methylpyridine-2-Carboxylate;2-Pyridinecarboxylic acid, 3-methyl-, ethyl ester;3-METHYL-2-PYRIDINECARBOXYLIC ACID ETHYL ESTER;SCHEMBL108857;DTXSID70482096;VKKVFRWNHZHHQU-UHFFFAOYSA-N;AM9817;AKOS011625752;AB64448;AC-23519;CS-11273;SY013318;A8314;CS-0061547;FT-0698648;3-Methylpyridine-2-carboxylic acid ethyl ester;EN300-195966;J-520891;3-METHYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER;Ethyl 3-Methylpyridine-2-carboxylate

Suppliers and Price of Ethyl 3-methylpyridine-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Ethyl 3-methylpyridine-2-carboxylate
25mg
$ 305.00

TRC
Ethyl3-methylpyridine-2-carboxylate
25mg
$ 45.00

Matrix Scientific
Ethyl3-methylpyridine-2-carboxylate 97%
1g
$ 179.00

Labseeker
Ethyl3-methylpyridine-2-carboxylate 95
50g
$ 492.00

Crysdot
Ethyl3-methylpicolinate 97%
10g
$ 335.00

Chemenu
Ethyl3-methylpyridine-2-carboxylate 97%
10g
$ 314.00

Apolloscientific
Ethyl3-methylpyridine-2-carboxylate 95%
10g
$ 129.00

Apolloscientific
Ethyl3-methylpyridine-2-carboxylate 95%
5g
$ 108.00

Apolloscientific
Ethyl3-methylpyridine-2-carboxylate 95%
25g
$ 228.00

American Custom Chemicals Corporation
ETHYL-3-METHYLPICOLINATE 95.00%
5MG
$ 501.50

Total 24 raw suppliers

Chemical Property of Ethyl 3-methylpyridine-2-carboxylate

Chemical Property:

Vapor Pressure:0.014mmHg at 25°C
Boiling Point:257.939oC at 760 mmHg
Flash Point:109.798oC
PSA：39.19000
Density:1.077g/cm3
LogP:1.56670
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:165.078978594
Heavy Atom Count:12
Complexity:159

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl 3-methylpyridine-2-carboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(C=CC=N1)C

Technology Process of Ethyl 3-methylpyridine-2-carboxylate

There total 4 articles about Ethyl 3-methylpyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4021-07-2
3-methyl-pyridine-2-carboxylic acid

: 64-17-5
ethanol

: 58997-10-7
ethyl 3-methylpyridine-2-carboxylate

Guidance literature:: With thionyl chloride; at 0 ℃; for 12h; Reflux;

Reference yield: 75.0%

: 20970-75-6
2-cyano-3-methylpyridine

: 64-17-5
ethanol

: 58997-10-7
ethyl 3-methylpyridine-2-carboxylate

Guidance literature:: 2-cyano-3-methylpyridine; With hydrogenchloride; water; Reflux;

ethanol; With sulfuric acid; Reflux;
DOI:10.1016/j.ejmech.2008.02.023

Reference yield:

: 1003-73-2
3-picoline-N-oxide

: 58997-10-7
ethyl 3-methylpyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 24 g / dimethyl sulphate / H₂O / 5 h / 80 °C

2: sodium hydroxide, water / 4 h / Heating

3: 70 percent / hydrogen chloride (gas) / 4 h / Heating

With hydrogenchloride; sodium hydroxide; water; dimethyl sulfate; In water;